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GCMS analysis results for unknown compounds, June 2002

Machine-extracted title · confidence 90%

Laboratory report documenting GCMS analysis of sample AE12738 with surrogate recovery data and identification of unknown compounds.

NYC-WTC_000015282–000015310

Folder label: “GCMS X 6/3/02 A 6/7/02

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Scanned page image, NYC-WTC_000015305
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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\MSDCHEM\1\DATA\060702\12739.D Vial: 15 Acq On 7 Jun 2002 7:58 pm Operator: Sample Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\060302.M (Cherns tat ion Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L

Peak Number 16 Phenanthrene, 9-methyl- Concentration Rank 18 R.T. EstConc Area Relative to ISTD R.T. 22.53 0.29 ug/L 345268 Phenanthranene-dl0 22.91 Hit# of 5 Tentative ID MW MolForm V CAS# Qua

1 Phenanthrene, 9-methyl- 192 C15H12 000883-20-5 53 2 Pyrazine, tetraethyl- 192 C12H20N2 038325-19-8 42 3 2-Propenal, 3-(3,4-dimethoxyphen... 192 C11H1203 4 Anthracene, 9-methyl- Abundance Scan 3311 (22.533 min): 12739.D (-3301) (-) 192 C15H12 004497-40-9 42 000779-02-2 40 m/z 192.00 100.00% W 192

5000

82 96 146 160 22.20 22.40 22.60 22.80

niz-> 0: TH—HHpmTTp- 40 51 70 । 118 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 l. rn/z 191.10 22.19% Abundance #81033: Phenanthrene, 9-methyl- 192

5000 22.20 22.40 22.60 22.80 m/z 146.10 14.17% 29 39 51 63 74 83 6 115 126 139 152 165 176 || Of IWTTOTTTIpmhmg ‘ I‘3 n/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #80990: Pyrazine, tetraethyl- 1912 177 / 22.20 22.40 22.60 22.80 5000 m/z96.00 13.44% 41 67

mz-> Abundance 0 29 uall.. 117 —m 53 .11 81 93 107 121 133 hmp । I 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 #80953:2-Propenal, 3-(3,4-dimethoxyphenyl)- 149 163 u 1912 22.20 22.40 22.60 22.80 161 m/z 193.00 12.96% 5000 77 121 149 177 91 103

m/z-> 0 m 52 64 U“ ‘ I' 138 al,.. al.. l.. 2030405060 70 8090 100 110 120 130 140 150 160 170 180 190 200 "i"" i 22.20 22.40 22.60 22.80

12739.D 060302.M Mon Jun 10 11:51:15 2002 Page 19

NYC-WTC_000015305

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NYC-WTC_000015305Source: NYC Law Department, mirrored locally

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