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← Document results/DEP Box 18/GCMS X 5/16/02 A 5/20/02
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GCMS scan data for sample AE11420, May 2002

Machine-extracted title · confidence 100%

Fragmented GCMS scan data page showing tentative identification of compounds and surrogate recovery for sample AE11420.

NYC-WTC_000025430–000025446

Folder label: “GCMS X 5/16/02 A 5/20/02

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Scanned page image, NYC-WTC_000025432
OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\MSDCHEM\1\DATA\052002\11420.D Vial : 10 Acq On : 20 May 2002 8:37 pm Operator: Mclean Sample : 5/16 eh Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L Peak Number 5 Phenanthrene, 9-methyl- Concentration Rank 11 R.T. EstConc Area Relative to ISTD R.T.

22.58 0.29 ug/L 403085 Phenanthranene-dl0 22.95

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Phenanthrene, 9-methyl- 192 C15H12 000883-20-5 53 2 Pyrazine, tetraethyl- 192 C12H20N2 038325-19-8 45/ 3 1,5-Naphthalenedithiole 192 C10H8S2 1000223-69-5 38 4 4-Hydroxy-3,5-dimethylcinnamic acid 192 C11H12O3 1000132-15-8 38 Abundance Scan 3319 (22.580 min): 11420.D (-3307) (-) m/ z 192.10 100/00%| 192

5000 - 82 96 146 160

miz—> 0 40 52 70 | 118 TWTITTtmmuawTo J | , 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 k 22.20 22.40 22.60 22.80 23.00 m/z 191.00 22.88% Abundance #81033: Phenanthrene, 9-methyl- 192

5000 22.20 22.40 22.60 22.80 23.00 m/z 193.10 15.59% 96 165 i । 29 39 51 63 74 83 l 115 126 139 152 j 176 . 0 TI’I"0103Tmm——d*T—umTTRTTTmT " i1 ‘ mfe-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #80990: Pyrazine, tetraethyl- 192 177 ......... ' I 1 1 1 ' I ’ 1 1 1 ' 1 i ■ ' 1 1 i ' 22.20 22.40 22.60 22.80 23.00 5000 m/ Z 96.10 13.48%| 41 67 53

mlz-> 0 4 29 | 81 93 107 121 133 TTtpmmmtT 149 163 7 I, I

20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 *T Abundance #80950:1,5-Naphthalenedithiole 192 22.20 22.40 22.60 22.80 23.00 m/z 146.10 11.83% 5000 115 128 159 40 57 69 79 96 147 -1 0- 11111111'l I anl, I r r l trrlpr#rppHrt=tpr. r 11 il-rp l 177 TTTTT TTp-r 11........ , /z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 22.20 22.40 22.60 22.80 23.00

11420.D 050102.M Thu May 23 14:07:11 2002 Page 8

NYC-WTC_000025432

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NYC-WTC_000025432Source: NYC Law Department, mirrored locally

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