GCMS analysis results, sample AE09154, May 2002

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Library Search Compound Report

Data File : C:\MSDCHEM\1\DATA\050902\9154.D Vial: 19 Acq On : 10 May 2002 6:47 am Operator: Mclean Sample : 5/8 eh Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\l\METHCDS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 8 Indolo[2,3-b]quinolizine, l.. Concentration Rank 17

R.T. EstConc Area Relative to ISTD R.T.

30.99 0.22 ug/L 186475 Chrysene-dl2 30.80 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Indolo[2,3-b]quinolizine, 1,2,3,. 240 C16H20N2 013233-45-9 9 2 3-Bromo-4-methoxyquinoline 237 C10H8BrNO 1000213-62-3 7 3 4(1H)-Quinazolinone, 2,3-dihydro... 238 C15H14N20 036384-00-6 7 4 Agroclavine 238 C16H18N2 000548-42-5 7 Abundance Scan 4751 (30.994 min): 9154.D (-4750) (-) m/z 239.10 100.00%| 239 86 106 117 5000

40 30.60 30.80 31.00 31.20 31.40 0— ' ' i ■ ■ ' ' i "rd m/ z 86.00 79.14%| n/z-> 40 60 80 100 120 140 160 180 200 220 240 Abundance #91178: lndolo[2,3-b]quinolizine, 1,2,3,4,6,7,12,12b-octah... 239

5000 AAAAAALAI 30.60 30.80 31.00 31.20 31.40 183 m/z 237.10 75.90%l 01 120 143 I ■ i ' ■ 1 159170 , ill 11 ll 1 i 1 '■ ■ i 1 ■ 194.211 1— Tl/Z-> 40 60 80 100 120 140 160 180 200 220 240 Abundance #90857:3-Bromo-4-methoxyquinoline 237

30.60 30.80 31.00 31.20 31.40 5000 194 m/z 106.05 69.78%| 115 50 62 74 88 101 128 .

n/z-> 01 1,0.1143158169181 , 298.27, ll, TTs 1mtr 1* 1 1tI" 1 T" I T " 40 60 80 100 120 140 160 180 200 220 240 Abundance #90849:4(1 H)-Quinazolinone, 2,3-dihydro1-methyl-3-phenyl- 237 30.60 30.80 31.00 31.20 31.40 m/z 83.90 68.71%|

5000 105 A 77 J 91 133

iz-> 51 0 1 ■ । ■ 1 ■ ■ । 40 60 ■ 0117 80 100 - 120 140 160 180 200 220 240 30.60 30.80 31.00 31.20 31.40

9154.D 050102.M Mon May 13 11:28:53 2002 Page 11

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