GCMS sample analysis results, AE11800, June 3, 2002

NYC 9/11 Public Portal Document

Library Search Compound Report Data’ File : C:\MSDCHEM\l\DATA\052202\11800.D Vial: 7 Acq On : 22 May 2002 6:43 pm Operator: Mclean Sample : 5/21 ad Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 10 Cyclotrisiloxane, hexamethyl-' Concentration Rank 14 R.T. EstConc Area Relative to ISTD R.T. 5.38 0.45 ug/L 304324 1,4-Dichlorobenzene-d4 9.90 Hit# of 5 Tentative ID MW MolForm CAS# Qua!

1 Cyclotrisiloxane, hexamethyl- 222 C6H1803Si3 000541-05-9 78 2 Cyclotrisiloxane, hexamethyl- 222 C6H1803Si3 000541-05-964 3 5-Methyl-2-phenylindolizine 207 C15H13N 036944-99-7 9 4 Cyclotrisiloxane, hexamethyl- 222 C6H1803Si3 000541-05-9 9 Abundance Scan 392 (5.383 min): 11800.D (-384) (-) m/z 207.05 1000.00% 2017

5000 ’ I*" I 96 191 ‘ 1 i 1 1 40 85 133 5.00 5.20 5.40 5.60 5.80 0 i ■ * ‘ • i * - 1i ■ • • ■ i ■ ■ ■ ■ I I m/z 208.0026.66% miz-> 0 20 40 60 80 100 120 140 160 180 200 Abundance #84874: Cyclotrisiloxane, hexamethyl- 207

5000 5.00 5.20 5.40 5.60 5.80 m/z 209.00 18.33% 96 133 _ 191 4 15 29 45 61 75 85. | . 119 । 147 163 177 L 0- 1Bnnp——n—m—a—B—pow’TTTTTPTTTTT ■ • । miz-> 0 20 40 60 80 100 120 140 160 180 200 Abundance #126480: Cyclotrisiloxane, hexamethyl- 207

5.00 5.20 5.40 5.60 5.80 5000 m/z 96.00 16.25%

96 28 45 61 75 86 0 T—nn——m—rTT . 1,106,119 133,147, 163 177.191 , ■ miz-> 0 20 40 60 80 100 120 140 160 180 200 Abundance #84865:5-Methyl-2-phenylindolizine 207 5.00 5.20 5.40 5.60 5.80 m/z 190.90 10.50%

5000

28 39 51 63 77 89 102 115 130 14 152 165 178 191 । 0 TI T1444I’III ■ ' i ■ ■ ■ ‘ i ■ • iz—> 0 20 40 60 80 100 120 140 160 180 200 5.00 5.20 5.40 5.60 5.80

11800.D 052202.M Tue May 28 12:04:36 2002 Page 13

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