GCMS results sample AE08256, April 2002

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Library Search Compound Report

Data File : C:\MSDCHEM\1\DATA\020417\08256.D Vial: 14 Acq On : 17 Apr 2002 8:12 pm Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1\METHODS\041702SCAN.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L Peak Number 8 Xenon Concentration Rank 5

R.T. EstConc Area Relative to ISTD R.T.

34.96 0.30 ug/L 345239 Perylene-dl2 34.79

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Xenon 132 Xe 007440-63-3 32 2 3-Pyridinecarbonitrile, 5,6-dime... 132 C8H8N2 113124-09-7 27 3 3,4-Dihydroisoquinoline 131 C9H9N 1000210-20-5 27 4 3-Phenyl-2-propyn-1-ol 132 C9H80 001504-58-1 22 Abundance Scan 5426 (34 960 min): 08256 D (-54 25) (-) m/z 130.10 100.00% 130

264 5000 55 96 115 193 208 34 60 34 80 35 00 35 20 36 73 0- -4 ■ ■ ।' 1 ■ ■ i ‘ ..................I n m/z 131.70 84.17% n/z-> 40 60 80 100 120 140160 180 200 220 240 260 Abundance #59698: Xenon 32

5000 34 60 34 80 35.00 35.20_______ 66 m/z 131.50 83.33% 0- .... i ..... .■ । n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 Abundance #59701: 3-Pyridinecarbonitrile, 5,6-dimethyH 11 .2

34.60 34 80 35.00 35.20 5000 m/z 264.15 58.00% 39 91 104 117 51 63 77 9 1 1 'T' 1 ' ' P I I n/Z-> 40 60 80 100 120 140 160 180 200 220 240 260 Abundance #58887 3,4-Dihydroisoquinoline 130 34 60 34 80 35.00 35 20_____ m/z 129.40 41.17% 5000- 103 51 77

39 i 65 ll 39 116 A . 0 — 1 i ' ■ 1 1 P ■ ■ ■ i 1 /Z—> 40 60 80 100 120 140 160 180 200 220 240 260 34 60 34 80 35 00 35.20

08256.D 041702SCAN.M Thu Apr 18 09:27:15 2002 Page 13

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