GCMS results for sample AE11566, May 29, 2002

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\MSDCHEM\l\DATA\020521\11566.D Vial: 17 Acq On : 22 May 2002 12:10 am Operator: Nefliu Sample : sample Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020521.M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1

Peak Number 4 Anthracene-diO- Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 31.96 0.34 ug/1 35700 Phenanthrene-dl0 31.72 Hit# of 5 Tentative ID MW MolForm CAS# Qual

' 1 Anthracene-diO- 188 C14D10 001719-06-8 33 2 Phe/ianthrene-dlO 188 C14D10 001517-22-2 16 3 Antipyrine 188 C11H12N2O 000060-80-0 9 4 Naphthalene, 1 z 7-dimethoxy-_________ 188 C12H1202 005309-18-2 9 Abundance Scan 4915 (31.958 min): 11566.D (-4906) (-) m/z 188.15 100.00% 188

5000 80 94 ■ i f■ r' > ■ > । • > ■ ■ । । । <

niz-> 0 ?,A4=l, mHmm 1’1" 10 20 30 40 50 60 70 80 90 100110 120 130 140 150 160 170 180 190 160 ll 31.60 31.80 32.00 32.20 m/z 80.10 23.83% Abundance #79826: Anthracene-d10- 188

5000 31.60 31.80 32.00 32.20 m/z 189.10 22.65% 80 94 160 . | 66 17 30 42 52 | 0 ''I................ I ■'' ■ I''" 111' mHTTt I 108118 132 146 +.79179/ Wt nz-> 10 20 30 40 50 60 70 80 90 100110 120 130 140 150 160 170 180 190 Abundance #79827: Phenanthrene-d10 188 TTT1 III4I11 31.60 31.80 32.00 32.20 5000 m/z 94.10 21.88%

A 80 94 160 30 42 52 66 11 108118 132 146 , |,| 170179.1,1 0-TIWWWTIWWTTTTTHTTHmimmphmtt n/z-> 10 20 30 40 50 60 70 80 90 100110 120 130 140 150 160 170 180 190 Abundance #125690: Antipyrine 1(18 31.60 31.80 32.00 32.20 m/z 184.20 20.30% 96 5000 77 56 105 43 67 1 115 129 159 173 ,| 0 1TI 1 . < I I . . 1 . I . m/z-> 10 20 30 40 50 60 70 80 90 100110 120 130 140 150 160 170 180 190 31.60 31.80 32.00 32.20

11566.D SCAN020521.M Fri May 24 09:40:07 2002 Page 6

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