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GCMS analysis results for sample AE11280, May 2002

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Laboratory report documenting GCMS analysis of sample AE11280 conducted on May 22, 2002, including surrogate recovery data.

NYC-WTC_000024730–000024742

Folder label: “GCMS X 5/13/02 A 5/15/02

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NYC 9/11 Public Portal Document Llbrary searen compound Keporc Data File : C:\MSDCHEM\1\DATA\020515\11280.D Vial: 14 Acq On : 16 May 2002 12:39 am Operator: Nefliu Sample : sample Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 ********************************************************************* Peak Number 6 Hexadecane, 1,16-dichloro- Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 38.53 0.58 ug/1 54713 Chrysene-dl2 39.93 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Hexadecane, 1,16-dichloro- 294 C16H32C12 007735-39-9 80 2 5-Tetradecene, (E) - 196 C14H28 041446-66-6 76 3 Hexadecanoic acid, 2-hydroxy-, m... 286 C17H34O3 016742-51-1 47 4 6-Tridecene, 7-methyl-_____________ 196 C14H28 024949-42-6 43 Abundance / Scan 6034 (38.532 min): 11280.D (-6027) (-) m/z 55.00 100.00% N 73 5000 97 wrdink na / M ct ■ । ■1 ■ i1' A..m.13777.. 191.., 196 330 - r I " ‘' I' " 1111'' 1 ‘ 1TTi . 11.(I 38.20 38.40 38.60 38.80 m/ z 69.10 76.53% m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 Abundance #14430: Hexadecane, 1,16-dichloro- 55 91 . /

5000 AMAAAAAAAA—MAaAar 71 38.20 38.40 38.60 38.80 29 m/z 43.10 72.90% 111 ■I ■ ■ * ’I 1, III 1..133 .161 189 215230 258 TTmwmt 294 ir ■ ■ ■ i i ■ * ■ ■ । miz-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 Abundance #13874:5-Tetradecene, (E)- wih, MWokr 38.20 38.40 38,60 38.80 5000 70 m/z 57.20 56.59% 29 97

—ll .1 112 139 168 196........... 1 , ’I . 11 . | ll . l| . I , . | . I , , I . . . r I , , , , ! , , I > | ! I I I | | ( | | | , , ! ! | I I ! I | I | ! | | m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 Abundance #13720: Hexadecanoic acid, 2-hydroxy-, methyl ester 55 38.20 38.40 38.60 38.80 83 m/ z 73.10 51.97% 29 5000

. 111 L LALii.127145 ' I ■'111 ’1’11111 TT1 1 i । ri 11 । r 1111 । i 227 286 ————— A TIT m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 38.20 38.40 38.60 38.80

11280.D SCAN020507.M Thu May 16 09:59:25 2002 Page 8

NYC-WTC_000024741

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NYC-WTC_000024741Source: NYC Law Department, mirrored locally

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