GCMS analysis results for sample AE08960, May 7, 2002

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Laboratory report documenting GCMS analysis of sample AE08960 conducted on May 7, 2002, by analyst DLV.

NYC-WTC_000049571–000049583

Folder label: “GCMS X 4/16/02 A 4/24/02”

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NYC 9/11 Public Portal Document

‘Data File : C:\MSDCHEM\l\DATA\020424\08960.D Vial: 11 Acq On : 24 Apr 2002 7:42 pm Operator: Nefliu Sample : sample Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020424.M (Chemstation Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 ********************************************************************* Peak Number 5 2,5-Dihydrophosphole, 3-met... Concentration Rank 6

R.T. EstConc Area Relative to ISTD R.T.

31.09 0.23 ug/1 430840 Phenanthrene-dl0 31.72

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 2,5-Dihydrophosphole, 3-methyl-l... 192 C11H13OP 1000196-97-5 45 2 1,5-Naphthalenedithiole 192 C10H8S2 1000223-69-5 36 3 Phenanthrene, 2-methyl- 192 C15H12 002531-84-2 28 4 Phenanthrene, 9-methyl- 192 C15H12 000883-20-5 28 Abundance Scan 4767 (31.088 min): 08960.D (-4750) (-) m/z 192.10 100.00% 19/2

5000

96 146 160 T-r-j-r-r 40 82 30.80 31.00 31.20 31.40

mfz~> I .49 TIWWIUINTT] .721. 1. l *• 2030405060 70 8090 100 110 120 130 140 150 160 170 180 190 200 109 ‘ ' I“• ’l“‘ ‘ I > 11111'111111(. |l p m/z 191.10 21.60% Abundance #80965:2,5-Dihydrophosphole, 3-methyl-1-oxo-1 -phenyl- 192 164

5000 99 115 30.80 31.00 31.20 31.40 47 77 177 m/z 146.10 19.16% 67 „ 125,34 146 miz-> -27 394+ ,57 .Il -5 HH 20 30 40 50 60 70 80 90 100110 120 130140150160 170180190 200 ‘ITT

Abundance #80950:1,5-Naphthalenedithiole 1:2

30.80 31.00 31.20 31.40 5000 m/z 193.10 19.04% 115 128 159 40 57 69 79 98 147 177 II’TT it. +4 i i1.1. । prrdemrtrrrpe 96 rep 1. hi r i lr 4TBOpuuor •>i•• mfe—> 20 30 40 50 60 70 80 90 100 110120 130140 150160170 180190 200 Abundance #125842: Phenanthrene, 2-methyl- • • • । •14 * rr * ‘48 **1’*’* 1:2 30.80 31.00 31.20 31.40 m/z 96.20 18.56%

5000

96 .

mfz-> 27 39 51 63 82 l 115 126 139 152 195 176 , . l.... ।... .‘I n 11 |i । n । i'i i r[ n । fl', r’l । I'l > । > ii । FUM 11111111111'| 1111 rrrp il'i 111 rHt 1111′1 B3ruur 20 30 40 50 60 70 80 90 100110120 130 140 150 160 170 180 190 200 -4 ■ i > ■ » • j ■ > 30.80 31.00 31.20 31.40

08960.D SCAN020424.M Thu May 02 14:44:29 2002 Page 7

NYC-WTC_000049581

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GCMS analysis results for sample AE08964, May 7, 2002 · Box DEP Box 27

NYC-WTC_000049622

Laboratory report documenting GCMS analysis of sample AE08964 conducted on May 7, 2002, by analyst DLV.

1 shared topics · Same agency, volume and box · similarity 0.998