GCMS analysis results for sample AE09156, May 2002

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Laboratory report documenting GCMS analysis of sample AE09156 conducted on May 8, 2002.

NYC-WTC_000046420–000046433

Folder label: “GCMS X 4/17/02 A 4/24 - 4/26/02”

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NYC 9/11 Public Portal Document

• Data File : C:\MSDCHEM\l\DATA\020424\09153.D Vial: 22 Acq On : 25 Apr 2002 6:29 am Operator: Nefliu Sample : sample Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e

Quant Method : C: \MSDCHEM\1\METHODS\SCAN020424 .M (Chemstation Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 ********************************************************************* Peak Number 6 2,5-Dihydrophosphole, 3-met.. Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T.

31.09 0.31 ug/1 620299 Phenanthrene-dl0 31.72 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2,5-Dihydrophosphole, 3-methyl-l... 192 C11H13OP 1000196-97-5 59 2 3-(2-Methoxy-5-methylphenyl)acry... 192 C11H1203 103986-76-1 50 3 4-Hydroxy-3,5-dimethylcinnamic acid 192 C11H1203 1000132-15-8 45 4 Anthracene, 2-methyl-_______________ 192 C15H12 000613-12-7 45 Abundance Scan 4768 (31.094 min): 09153.D (-4758) (-) rn/z 192.10 100.00% 19/2

_ / 5000 40 96 ■ ■ i ■ ■ 82 146 160 30.80 31.00 31.20 31.40 51 70 + .'‘i .^'l 111" ■ ।" i1"111 tr 1111‘|' ।' 11 > 11' । ■ | 1,11" 11" " r ' . ........... I'1' m/ z 40.10 38.79% n/z—> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #80965: 2,5-Dihydrophosphole, 3-methyl-1-oxo-1 -phenyl- 192 164

5000 99 115 30.80 31.00 31.20 31.40 47 77 177 m/Z 191.10 24.67% 67 125,34 146 27 3?, 4.57p, +7+444l++4155, m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #80954: 3-(2-Methoxy-5-methylphenyl)acrylic acid 161 1912

30.80 31.00 31.20 31.40 5000 105 m/z 96.10 17.62% 77 132 91 115 145 39 51 65

m/z-> ' i " " i' " l/r o 1 r r Mr,, ll H %...fl.......... /.... 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #81030: 4-Hydroxy-3,5-dimethylcinnamic acid ■ ' i ' ' ■ ' i ■ ' 192 30.80 31.00 31.20 31.40 m/ Z 160.20 11.05% 5000

89 175 63 145 45 I 77 105 117 135 ---TTTTTTTTTTTT li 163 |,|||l"l‘l I'11'11'111i'i1111'■ । TI’T n/z—> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 30.80 31.00 31.20 31.40

09153.D SCAN020424.M Fri May 03 11:00:31 2002 Page 8

NYC-WTC_000046431

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GCMS analysis results for sample AE09153, May 2002 · Box DEP Box 27

NYC-WTC_000046405

Laboratory report documenting GCMS analysis of sample AE09153 conducted on May 8, 2002.

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