NYC-WTC_000046420
Laboratory report documenting GCMS analysis of sample AE09156 conducted on May 8, 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗Document / 15 pages
GCMS analysis results for sample AE09153, May 2002
Machine-extracted title · confidence 100%Laboratory report documenting GCMS analysis of sample AE09153 conducted on May 8, 2002.
NYC-WTC_000046405–000046419Folder label: “GCMS X 4/17/02 A 4/24 - 4/26/02”
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NYC 9/11 Public Portal Document
Data File : C:\MSDCHEM\l\DATA\020424\09152 .D Vial: 21 Acq On : 25 Apr 2002 5:30 am Operator: Nefliu Sample : sample Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e
Quant Method : C:\MSDCHEM\1\METHODS\SCAN020424.M (Chemstation Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1
Peak Number 7 Bisvertinol Concentration Rank 3
R.T. EstConc Area Relative to ISTD R.T.
44.52 0.78 ug/1 1000460 Perylene-dl2 43.15
Hit# Of 5 Tentative ID MW MolForm CAS# Qual
1 Bisvertinol 498 C28H3408 1000145-05-4 16 2 5.alpha.-Pregnan-20-one, 12.beta... 318 C21H3402 005618-22-4 12 3 Isodihydrobisvertinol 500 C28H3608 1000143-59-2 10 4 IH-Isoindole-l,3(2H)-dione, 3a,6... 257 C15H15NO3 054346-14-4 9 Abundance Scan 7053 (44.520 min): 09152. D (-7040) (-) m/z 40.10 100.00% 43
95 5000 124 149 215 67
n/z->50 100 khkai 248 150 200 Il 281 250 300 216 316 350 373
400 450 500 44.20 44.40 44.60 44.80 m/z95.10 55.32% Abundance #41009: Bisvertinol
_wth 43 95
5000 67 217 44.20 44.40 44.60 44.80 149 m/ Z 43.10 51.86% .123 191 ul100I1 1l ' 150ulL 250
Wu ■ ' i -------------- m/z-> 50 200 250 300 350 400 450 500 Abundance #5096: 5.alpha.-Pregnan-20-one, 12.beta.-hydroxy- 43 . ' ' I 1 ' ' ' I ' ' ’ ' I ' ' ' ' I ' ' ' ' I 44.20 44.40 44.60 44.80
N 5000 m/ Z 55.10 49.18% 81 | 109 242 149 300 — al 4 1,41 r1 215 1 267 | . 190— 11 -r-j-r •n/z—>_______ 50 100 150 200 250 300 350 400 450 500 Abundance #4606: Isodihydrobisvertinol . 1 43 181 44.20 44.40 44.60 44.80 95 67 m/ Z 93.00 42.77% 217 5000 136
/z—> T 50 100 150 IL 200 251 I 250 300 ..................................... 482 350 400 450 500 44 aku 44.20 44.40 44.60 44.80
09152.D SCAN020424 .M Fri May 03 10:59:33 2002 Page 9
NYC-WTC_000046417
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NYC-WTC_000046417Source: NYC Law Department, mirrored locally
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NYC-WTC_000044119
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