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GCMS analysis results for sample AE09153, May 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AE09153 conducted on May 8, 2002.

NYC-WTC_000046405–000046419

Folder label: “GCMS X 4/17/02 A 4/24 - 4/26/02

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NYC 9/11 Public Portal Document

'Data File : C:\MSDCHEM\1\DATA\020424\09152.D Vial: 21 Acq On : 25 Apr 2002 5:30 am Operator: Nefliu Sample : sample Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020424.M (Chemstation Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 ****************************************************************** ** * Peak Number 8 2-(l-Cyano-3-methylbut-2-en... Concentration Rank 7

R.T. EstConc Area Relative to ISTD R.T.

44.78 0.31 ug/1 395465 Perylene-d12 43.15

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-(l-Cyano-3-methylbut-2-enylami... 203 C12H17N3 1000191-53-7 4 2 Benzofuran, 7-(2,4-dinitrophenox... 374 C18H18N2O7 062059-46-5 4 3 (-)-cis-Myrtanylamine 153 C10H19N 038235-68-6 2 4 Benzeneethanamine, 4-fluoro- 139 C8H10FN 001583-88-6 1 Abundance Scan 7098 (44.784 min): 09152.D (-7085) (-) m/z —RAARKww~ 40.10 100.00% 43

5000

467 22 721 142161 207 231 281 ............. I___________ 1 iTrjr TT rp I V I | I T> I p r n | YY I r I I I I I । I I i I I r I H | I i I i | I I I ' i" " i"'111 ■11 r 386 _______________ 1 I" ’' I" " I"'' 44.40 44.60 44.80 45.00 45.20 m/ Z 43.10 22.45% rn/z-> 0 20 40 60 80 100 120 140160180 200 220 240 260 280 300 320 340 360 380 A Abundance #72: 2-(1-Cyano-3-methylbut-2-enylamino)-4-methylpent-3-en...

w/Wmusu 27 67 94 176 5000 44.40 44.60 44.80 45.00 45.20 . 136 m/ z 41.20 15.44%

m/z-> mAeala,a,Lise. i"'111" 1 r " ■ i11" 11 i ri 11111111111111111111 [" 111111 0 20 40 60 80 100 120140 160 180 200 220 240 260 280 300 320 340 360 380 Abundance #426: Benzofuran, 7-(2,4-dinitrophenoxy)-3-ethoxy-2,3-dihy... 29 4 ‘ 1 | 1 'T 1 | 1 1 44.40 44.60 44.80 45.00 45.20 AMM 5000 m/Z 93.20 15.27% 79 133 51 . 107

n/z-> ..441478, 161179 207225243 280 303 329 11—mDummmPTT 0 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 374

Abundance 33 #733: (-)-cis-Myrtanylamine 14 441,,. I 44.40 44.60 44.80 45.00 45.20 m/Z 107.20 13.71% 5000

TI ......................................................................................................... A 1Ak........ I...... ■ ] ■ ■ ■ ■ | -> । -i-i । । "i । । । । । n/z-> 0 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 44.40 44.60 44.80 45.00 45.20

09152.D SCAN020424 .M Fri May 03 10:59:36 2002 Page 10

NYC-WTC_000046418

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NYC-WTC_000046418Source: NYC Law Department, mirrored locally

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