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GCMS analysis results for sample AE10160, May 2002

Machine-extracted title · confidence 90%

Laboratory report showing GC/MS analysis results for sample AE10160 including surrogate recovery data on May 14, 2002.

NYC-WTC_000023454–000023471

Folder label: “GCMS X 5/9/02 A 5/13/02

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NYC 9/11 Public Portal Document

• Data File : C:\MSDCHEM\1\DATA\051302\10160.D Vial: 10 Acq On : 13 May 2002 6:49 pm Operator: Mclean Sample : 5/9 kb Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L

Peak Number 7 Anthracene, 2-methyl- Concentration Rank 5

R.T. EstConc Area Relative to ISTD R.T.

22.58 0.27 ug/L 312982 Phenanthranene-dl0 22.95

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Anthracene, 2-methyl- 192 C15H12 000613-12-7 64 2 Phenanthrene, 9-methyl- 192 C15H12 000883-20-5 53- 3 Anthracene, 9-methyl- 192 C15H12 000779-02-2 50- 4 5H-Dibenzo[a,d]cycloheptene 192 C15H12 000256-81-5 45 Abundance Scan 3319 (22.580 min): 10160.D (-3306) (-) m/z 192.10 100.00% 192

5000 ,... .............. 146 160

mfe-> 04 111 ‘' ] 49 nmmhp mmp 70 82 96

20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 118 HHH L 22.20 22.40 22.60 22.80 23.00 m/Z 191.10 21.73%

Abundance #125845: Anthracene, 2-methyl- 192

5000 22.20 22.40 22.60 22.80 23.00 m/z 193.10 17.32% 66 75 87 96 115 126 139 152 165 1/6 O- i"111"111" " i" " i11’l*i i'1'11’l11 MIT*11 r''1'11 ITtT > 111'| > 111 |'i... । i'i'i . ।. r’l’t ।.. .'i1 Tg m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #81033: Phenanthrene, 9-methyl- 192 ..... ........ jy 22.20 22.40 22.60 22.80 23.00 5000 m/z 146.10 13.41% fl 96 165 । । 29 39 51 63 74 83 J 115 126 139 152 1 176 1 0 TITTTTLUTTTLTTTTLTTTTTTTTTTTTTTTHTUTTTETTTTTTTPTTTTTTTTTTTTNTT 111 n/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #125848: Anthracene, 9-methyl- ,12.. 192 22.20 22.40 22.60 22.80 23.00 m/ z 96.10 11.60%

5000

96 EE 27 39 51 63 82 | 115 126 139 152 ? 176 „ 0 11" " 11' "'I " " I'" " 11,1" I..... I'1 ■ rM 11" " I' 1IITT 11 ■ n'l " " I'11" 1111' 1" 111 "11 11’1 1 1 ‘ * 1 ' I ' ' ' 1 i ■ ■ 1 ■ i ' m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 22.20 22.40 22.60 22.80 23.00

10160.D 050102.M Tue May 14 11:40:50 2002 Page 10

NYC-WTC_000023468

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NYC-WTC_000023468Source: NYC Law Department, mirrored locally

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