GCMS Method 508 scan results, April 2002

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- Data File : C:\MSDCHEM\1\DATA\020419\08487.D Vial: 24 Acq On : 20 Apr 2002 6:46 am Operator: Ne fliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020418.M (Chemstation Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1

Peak Number 9 Anthracene-dlO- Concentration Rank 6 R.T. EstConc Area Relative to ISTD R.T. 31.95 0.42 ug/1 817855 Phenanthrene-dl0 31.72 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Anthracene-dlO- 188 C14D10 001719-06-8 50 2 Cyclohept anone, 4-phenyl- 188 C13H160 067688-28-2 47 3 Pentacyclo[8.4.0.0(3,7).0(4,14).... 188 C14H20 1000099-27-2 36 4 4-Methyl-2-(4-fluorophenyl)pyrim. .. 188 C11H9FN2 076128-67-1 33 Abundance Scan 4914 (31.952 min): 08487.D (-4898) (-) m/z 188.20 100.00%| 1(18

5000

80 94 TII T1 1 ^1 1 1 1 1 I 1 1 1 1 1 1 31.60 31.80 32.00 32.20 40 66 | ]| 106 146 160 mlz-> 0 ' i'" 'I"'' r ” ■!'11 ‘i"' ■ i ■11 'i1 ■ mmmph 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200210 117/1111/297/11 m/z 94.20 15.84%| Abundance #79826: Anthracene-d10- 188

................................................. 5000 31.60 31.80 32.00 32.20 m/ z ,80.20 12.76 80 94 160 ,1 66

z-> 0 17 30 42 52 ''I'"' I'...... . -HH | J 108118 132 146 I" "IHl 'l" "i1""I ।" 'I" 1.1 ■ 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200210 +179.4 TTInguum Abundance #79739: Cycloheptanone, 4-phenyl- 1(8 117 104 ’T 91 160 31.60 31.80 32.00 32.20 5000 131 m/z 184.10 11.23%| 170 145 ... n... r, . ■ rern । mreep r, A „ l A | 41 nil 41 All, 11A J. 4 ailijirya 0- mtz-> 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200210 Abundance #79714: Pentacyclo[8.4.0.0(3,7).0(4,14).0(6,11)]tetradecane "IT i ‘ ■ ■' ।11 * * । *1 • ।1 188 31.60 31.80 32.00 32.20 m/Z 189.10 ii.io%| 5000 79 91 100 117 131 10 41 FF 67 Ol ) ”7’ 145 1 159 1 173 "i^ । 0 rmp * ,,, 1hrtpall ,, mhl , ,l|l|l| i, i ll । All, , ,'|l|l|l|-,, , ।, ,l|l, ।,,, 1 npnp l .... ।. 11., r "T । ■ ■ ■1 । ■ 1 1 1 i 1 1 1 1 ।1 n/z-> 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200 210 31.60 31.80 32.00 32.20

08487.D SCAN020418.M Mon Apr 29 08:36:52 2002 Page 27

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