Laboratory report of a GCMS blank run conducted on May 14, 2002, showing non-detect results for various compounds.
NYC-WTC_000022965–000022989Folder label: “GCMS X 5/8/02 A 5/9/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document LLDrdLY sect run compourC Report
Data File C:\MSDCHEM\1\DATA\050902\0508LB.D Vial: 4 Acq On 9 May 2002 5:43 pm Operator: Mclean Sample 5/8 kb Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\l\METHCDS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 6 3-Pyrrolidinol Concentration Rank 13
R.T. EstConc Area Relative to ISTD R.T.
7.74 0.25 ug/L 197251 1,4-Dichlorobenzene-d4 9.94
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 3-Pyrrolidinol 87 C4H9NO 040499-83-0 9 2 5-Hexen-2-one 98 C6H10O 000109-49-9 9 3 2 -Propanone, 1-eye1opropy1- 98 C6H10O 004160-75-2 9 4 Acetone______ 58 C3H60 000067-64-1 7 Abundance Scan 793 (7.738 min): 0508LB.D (-784) (-) m/z 43.10 100.00%
K 43
5000 alywaw 58 87 ■ ■ i 1 ■ ■ ■ i ' ■ ■ ' I ■ ‘ ‘ ■ I
49 . 98 7.40 7.60 7.80 8.00 0 11"' I" " 11 ‘" I' ■'' I' ‘‘ I" " I"''I I'II1 >11>111'11!111H11'111। । । b 11. । ■ mmmmm m/z 58.10 24.01% m/z-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 Abundance #4163: 3-Pyrrolidinol 40 ul Wupoku 5000 1 1 i ■ ' 1 ■ i ' ■ ■ ■ i 1 ' ' 1 I ■ ' ' ' i 7.40 7.60 7.80 8.00 57 87 m/z 87.00 16.69% 68
m/z-> 0 11’11011111"0111311111023 —1011113TT ...... . -TTT 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 ll... .. Abundance #109454:5-Hexen-2-one 40 1 ■ i 1 ■ ' ■ i 7.40 7.60 7.80 8.00 5000 m/z 59.00 10.93% 55
0 --+-32. 15 27 38.+ 50 63 71 77 83 98 11111111111 I | t 11 I ri i ] TTpi i T|-nr I | . I I . | I I I I | . I I I | . 11 11 I I I . | . A nz-> Abundance 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 #5149: 2-Propanone, 1-cyclopropyl- 40 ■ ■ I ' 1 - • I ‘ ' 7.40 7.60 7.80 1....... 8.00 m/z 83.00 9.55%
5000
55 27 69 83 98 0 IT mmmmHhm 111111111 l| 11 59. 11 +TTTTTTTTmmpmgTgu ‘ ■ i ■ ■ ■ 1 i m/z-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 7.40 7.60 7.80 8.00
0508LB.D 050102.M Tue May 14 10:14:53 2002 Page 9
NYC-WTC_000022977
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NYC-WTC_000024041
Laboratory report showing non-detectable levels of nitrosamines and other contaminants in blank sample AE10895.
1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000025216
Laboratory report showing GCMS blank analysis for sample AE11410 conducted on May 22, 2002.
1 shared topics · Same agency, volume and box · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000023409
Laboratory report showing non-detect results for volatile organic compounds in a method blank sample AE10137 analyzed on May 14, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.992
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000023925
Laboratory report showing GC/MS analysis of sample AE10982 with surrogate recovery data for 2,4-DDD.
1 shared topics · Same agency, volume and box · similarity 0.992
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000023991
Laboratory report showing GC/MS analysis of sample AE10984 with surrogate recovery data for 2,4-DDD.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.991
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000025102
Laboratory report showing GCMS analysis results for sample AE11381 conducted on May 22, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.991
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000023949
Laboratory report showing GC/MS analysis of sample AE10983 with surrogate recovery data for 2,4-DDD.
1 shared topics · Same agency, volume and box · similarity 0.991
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000045936
Gas chromatography-mass spectrometry blank analysis conducted May 17, 2002 testing for semivolatile organic compounds with all results below method reporting limits.
1 shared topics · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000044559
Laboratory report showing blank test results for various organic compounds on May 7, 2002.
1 shared non-person entities · 1 shared topics · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000013883
Fragmented document header from DEP Box 15 archive containing metadata for environmental testing records dated late May 2002.
1 shared topics · similarity 0.991
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000046006
Gas chromatography-mass spectrometry report for sample AE10810 showing detection of unknown compounds and surrogate recovery.
1 shared non-person entities · 1 shared topics · similarity 0.991
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000044381
Gas chromatography-mass spectrometry blank analysis showing results below method detection limits for organic compounds.
1 shared topics · similarity 0.991
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000022961
Department of Environmental Protection administrative record sheet for World Trade Center site activities dated May 2002.
Filed in the same folder
NYC-WTC_000022962
Fragmentary record containing a document identifier and date from the DEP GCMS analysis series.
Filed in the same folder
NYC-WTC_000022990
Laboratory report documenting GCMS calibration verification analysis conducted on May 14, 2002.
Filed in the same folder
NYC-WTC_000022994
Laboratory report of GCMS reference standard analysis conducted on May 14, 2002, showing recovery percentages.
Filed in the same folder
NYC-WTC_000023002
Fragmentary record containing a document identifier and date from the DEP GCMS analysis series.
Filed in the same folder