GCMS analysis results for sample AE10897, May 21 2002

NYC 9/11 Public Portal Document

Data File : C:\MSDCHEM\1\DATA\051602\10897.D Vial: 10 Acq On : 16 May 2002 9:52 pm Operator: Mclean Sample : 5/10 eh Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\l\METHCDS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L Peak Number 3 3-Pyrrolidinol Concentration Rank 5 R.T. EstConc Area Relative to ISTD R.T. 7.74 0.23 ug/L 171020 1,4-Dichlorobenzene-d4 9.93 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3-Pyrrolidinol 87 C4H9NO 040499-83-0 37 2 4-Penten-2-one, 4-methyl- 98 C6H10O 003744-02-3 17 3 Acetone 58 C3H60 000067-64-17 4 Acetone 58 C3H60 000067-64-1 7 Abundance Scan 793 (7.739 min): 10897.D (-781) (-) m/ z 43.10 100.00% 43

5000 MWwWAww 58 39 87 1 ■ i ■ ■ ■ ■ । ■ ■ ■ ■ । ■ 1 ' ■ । ■ ■ ' ■ । 98

m/z—> 0- ........... Ii/7II mm 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 83 m 7.40 m/ z 7.60 58.10 7.80 8.00 26.11% Abundance #4163:3-Pyrrolidinol 43

*MHPMM 5000 7.40 7.60 7.80 8.00 57 68 87 m/ z 87.00 18.47%

m/z—> 0 47.5211 .... 1' i " " I " " i" " I " " Iill 77 83 I1"'I'"4"" THTTTTTTTT 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #110033:4-Penten-2-one, 4-methyl- 43 ■ ' i ' ' ' ■ i 7.40 7.60 7.80 8.00 5000 m/z 57.10 14.89%

83 28 32 38 98

m/z—> Abundance 0 1 ■ i ■' 55 ■ i ■ i J < [ 11111 ‘ ।11 ■ • > n 111111' 1111'

15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 s #109707: Acetone । 1 1 ■ • । 43 7.40 7.60 7.80 8.00 m/ z 39.10 13.97%

5000 58 27 0 —++31—34—4 TP 111"' r " 1 r 1" i1"111" 11" " I " " r "11" " 111 ' i ' । । 1 i 1 ' 1 ’ i 1 । mi 1 1 ' । m/z—> 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 7.40 7.60 7.80 8.00

10897.D 050102.M Fri May 17 15:05:38 2002 Page 5

NYC-WTC_000024109