GCMS analysis results for sample AE10163, May 2002

NYC 9/11 Public Portal Document

* Data File : C:\MSDCHEM\1\DATA\051302\10163.D Vial: 11 Acq On : 13 May 2002 7:38 pm Operator: Mclean Sample : 5/9 kb Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\l\METHCDS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L Peak Number 3 3-Pyrrolidinol Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T.

7.73 0.31 ug/L 261382 1,4-Dichlorobenzene-d4 9.93

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3-Pyrrolidinol 87 C4H9NO 040499-83-0 35 2 2-Hexanone, 5-methyl- 114 C7H140 000110-12-3/33 3 Acetic acid ethenyl ester 86 C4H602 000108-05-4 9 4 2,3-Dihydrooxazole, 2-t-butyl-4-... 98 C6H10O 036808-01-2 9 Abundance Scan 792 (7.733 min): 10163.D (-786) (-) m/ z 43.10 100.00% 43

5000 58 MAN 1 ' I ' ' ' 1 I ' ’ ' 1 I I 87 98...................... .................................. 7.40 7.60 7.80 8.00 0- m/ z 58.10 38.73% m/z-> 0 10 20 30 40 50 60 70 80 90 100 110 120 Abundance #4163: 3-Pyrrolidinol 43 Mar 5000 ■ ' । ■ ' ' ' । 7.40 7.60 7.80 8.00 87 m/ z 41.20 18.38% 57 68 511/1/1/177 0- ■ ■ । . ■ • • । ■ ■ ■ ■ । ■ ■ ■ ■ । ■ > ■ > । > +PT miz-> 0 10 20 30 40 50 60 70 80 90 100 110 120 Abundance #109705: 2-Hexanone, 5-methyl- 43 7.40 7.60 7.80 8.00 5000 m/z 87.10 16.98% 58 27

n/z-> 01 -l PTTT50 ulll 0 10 20 30 40 60 71 L 70 80 85....... 99........ 114 90 100 110 120 Abundance #3867: Acetic acid ethenyl ester ‘ ' I ' ' ' ' I ' ' ‘ 1T 1 ' ' ' I ' ' ' ' I 43 7.40 7.60 7.80 8.00 m/z 83.00 16.53% 5000 15

—4p20 l 27 86

miz-> 0 010 30 37 , 40 I 50 60 70 80 90 100 110 120 7.40 7.60 7.80 1 1 i ‘ 8.00 ■ 1 ।

10163.D 050102.M Tue May 14 11:41:24 2002 Page 6

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