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← Document results/DEP Box 18/GCMS X 5/8/02 A 5/9/02
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GCMS analysis results for sample AE09577, May 2002

Machine-extracted title · confidence 90%

Laboratory report showing GCMS analysis of sample AE09577 conducted on May 14, 2002.

NYC-WTC_000023179–000023194

Folder label: “GCMS X 5/8/02 A 5/9/02”

←Page 13 of 16→
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NYC 9/11 Public Portal Document

, Data File : C:\MSDCHEM\1\DATA\050902\9577.D Vial: 13 Acq On : 10 May 2002 1:04 am Operator: Mclean Sample : 5/8 kb Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\l\METHCDS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L

Peak Number 5 3-Pyrrolidinol Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

7.73 0.32 ug/L 265790 1,4-Dichlorobenzene-d4 9.94

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3-Pyrrolidinol 87 C4H9NO 040499-83-0 37 2 5-Hexen-2-one 98 C6H10O 000109-49-9 9 3 Methyl 1-methylcyclopropyl ketone 98 C6H10O 001567-75-5/9 4 4-Penten-2-one, 4-methyl- 98 C6H10O 003744-02-/ 9 Abundance Scan 792 (7.733 min): 9577.D (-786) (-) m/ z 43.10 100. 00% 43

5000 58 87 ' 1 1 1 1 1 ' I ■ ' ' ' I ' ' 1 1 I 7.40 7.60 7.80 8.00 01 I " " I " " I"' '1" “ I " " I" " I" '' I " I'1" - m/z 58.10 30.53% m/z-> I5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 Abundance> #4163: 3-Pyrrolidinol 43 j v-ALmmka MAMwAHM 5000 J ■ ■ i ■ ■ ■ ■ i ■ ■ ■ ■ i ■ ' ■ 1 i ■ ■ ' 1 i

7.40 7.60 7.80 8.00 57 87 m/z 87.10 17.79% 68 0 i" " i" "i ■■ "i" " i1 ‘" i"" r ■ ■■ i 111.521/ Appill .P''11'77"11'" 82 11,1 " i 110211111119111 n/z-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105

I Abundance #109457:5-Hexen-2-one 43 ’ I’’ b ■ । ■ T" I ' 1 1 1 1 7.40 7.60 7.80 8.00 5000 m/z 57.10 15.42%

55 2711111 ■ 11. 38 0 I ■"' I" " I' ■ । ■ 11111111 I 50 , 65 71 77. 83 98 । il 111 TTT 111"111" ।' i" " i" " n/z-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 Abundance #5005: Methyl 1 -methylcyclopropyl ketone ————— 17.3 n 43 7.40 7.60 7.80 8.00 m/z 41.10 15.25% N 5000 55 29 83 98

n/z-> 15 0 plapani).....+L3A++ 50 , 63 69 77 | || 11111111111 j 11 TT-p-TTTpTTTp-|T-|TrTTTpT+rp-|TTT^^ 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 7.40 7.60 7.80 8.00

9577.D 050102.M Mon May 13 11:52:25 2002 Page 8

NYC-WTC_000023191

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NYC-WTC_000023191Source: NYC Law Department, mirrored locally

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