GCMS analysis results for sample AE09577, May 2002

NYC 9/11 Public Portal Document

’ Data File : C:\MSDCHEM\1\DATA\050902\9577.D Vial: 13 Acq On : 10 May 2002 1:04 am Operator: Mclean Sample : 5/8 kb Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L Peak Number 4 2-Pentanone, 4-hydroxy-4-me... Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T. 5.97 14.74 ug/L 12230900 1,4-Dichlorobenzene-d4 9.94

Hit# of 5 Tentative ID MW MolForm CAS# a

l 2-Pentanone, 4-hydroxy-4 -methyl- 116 C6H12O2 000123-42-2 6 2 2-Pentanone, 4 -hydroxy-4 -methyl- 116 C6H12O2 000123-42-2 72 3 2-Pentanone, 4-hydroxy-4-methyl- 116 C6H1202 000123-42-2 64 4 Acetone______ 58 C3H60 000067-64-1 32 Abundance Scan 492 (5.970 min): 9577.D (-485) (-) m/ z 43.10 100.00% 43

5000 59 101 560 5.80 6.00 6.20 6.40

miz-> ol .............. 10 20 30 37,11 40 +53+ 50 119125 67 83 , | 11 1 ' 1 i ■ ■ ■ 1 i 1 1 ■ ■ i ' 1 ' 1 i 1 ' 1 ■ i ■ ■ ’ ■ i 1 ' 1 ' i ■ ‘ 60 70 80 90 100 110 120 130 m/z 59.10 34.00%

Abundance #109755: 2-Pentanone, 4-hydroxy-4-methyl- 43

5000 59 560 5.80 6.00 6.20 6.40 m/z 58.05 21.29% 15 101

mlz~> 01 ■ ■ I ' 10 ,25131,371 20 30 40 +53+ 50 83 , | 1uwaIa*uu‘wuajala-/0180*/* 60 70 80 90 100 110 120 130 Abundance #109756:2-Pentanone, 4-hydroxy-4-methyl- 43 560 5.80 6.00 6.20 6.40 5000 59 m/z 101.10 13.86%

93 101 83 — 93 n/z-> 01 ...... 10 20 25131.37, 30 40 I-' H 50 । I 1 ' ■ ■ i 1 ■ 1 ' i 1 ' r ■ i ■ ■ 1 1 i ' ■ ■ ■ i ■ ■ ■ ■ i ■ ■ ■ ■ i ' ■

60 70 80 90 100 110 120 130 Abundance #5851:2-Pentanone, 4-hydroxy-4-methyl- 43 5 60 5.80 6.00 6.20 6.40 m/z 41.05 5.54%

5000 59 27 37 . 101 67 77 83 91 । 0 ---44 53 H ' I'''''1 I ■ ■ ■ ' i ■ ' 1 ■ i ■ ' ■ ' i ' ' ■ 1 i 1 ' ' 1 i ‘ ' ■ ■ i ' ' 1 1 i ' ' TT । । , PP PTTT miz-> 10 20 30 40 50 60 70 80 90 100 110 120 130 5.60 5.80 6.00 6.20 6.40

9577.D 050102.M Mon May 13 11:52:24 2002 Page 7

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