GCMS analysis results for sample AE12474, June 2002

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Laboratory report documenting gas chromatography-mass spectrometry analysis of environmental sample AE12474 conducted on June 4, 2002.

NYC-WTC_000014102–000014124

Folder label: “GCMS X 5/24/02 A 5/28/02”

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NYC 9/11 Public Portal Document UJLCLY DEdICI LoLIpOLIIC KCDOIC

Data File : C:\MSDCHEM\l\DATA\052802\12474.D Vial: 12 Acq On : 28 May 2002 11:15 pm Operator: McLean Sample : 5/24 ad Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\052202.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 14 Anthracene -d10- Concentration Rank 9

R.T. EstConc Area Relative to ISTD R.T. 23.06 0.29 ug/L 272730 Phenant hranerie - dl 0 22.91

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Anthracene-dlO- 188 C14D10 001719-06-8 93 2 Phenanthrene-diO 188 C14D10 001517-22-2 80 3 Pentacyclo[7.3.1.1. (4,12) .0(2,7) ... 188 C14H20 1000215-61-8 42 4 2-Quinolinecarboxaldehyde, 8-hyd. . . 188 C10H8N2O2 005603-22-5 38 Abundance Scan 3401 (23.062 min): 12474.D (-3393) (-) m/z 188.10 100.00% 188

5000

80 94

niz-> 0 mmmTTT 43 „74 — 66 — Hmmmmmmmmm i - ‘1 ■ 158

10 20 30 40 50 60 70 80 90 100110120130140150160 170180190 m/z 22,80 23.00 23.20 23.40 94.10 19.66% Abundance #79826: Anthracene-d10- 188

,1 5000 22.80 23,00 23.20 23.40 m/z 189.10 16.83% 80 94 160 , 17 30 42 52 P . . 108118 132 146 11. 170179.1,। | 0J 111 ■ 111111 11 < 111111111111111! 111111111 it t*| 111 j p t i 1111 i t j 1111 p 111 p > 11 p I Pip t i i p 1111PPI 1i111 iz-> 10 2030405060 70 8090 100110120130140150160170180190 Abundance #79827: Phenanthrene-d10 188

'' 22.80 23.00 23.20 23.40 5000 m/z 80.10 16.29%

80 94 160 42 ■111 30 11111 521111111 66■ 111 PI, 11111 H108118 132 146 11 170179,1.1 I 0 1111 ‘' I ‘1'1 i'' i l p 11 j p 111 p i i i p l 11 p i l q 11 l ip "’l’l’’ iiipin|1’lIp un niz-> Abundance 10 20 30 40 50 60 70 80 90 100110120130140150160170180190 #79715: Pentacyclo[7.3.1.1.(4,12).0(2,7).0(6,11)tetradeca... 188 —A 22.80 23.00 23.20 23.40 m/z 184.20 14.81% 5000 79 91 55 67 105 117 131 145 159 0— ...... ’1’11912103310 ’0112’I— 1331" +4----p— 1’173 .. Il.. 1411-4414451 - miz-> 10 20 30 40 50 60 70 80 90 100110120130140150160170180190 22.80 23 00 23.20 23.40

12474.D 052202.M Thu May 30 10:43:02 2002 Page 17

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GCMS analysis results for sample AE12472, June 2002 · Box DEP Box 15

NYC-WTC_000014054

Laboratory report documenting gas chromatography-mass spectrometry analysis of environmental sample AE12472 conducted on June 4, 2002.

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