GC/MS analysis results for sample AE11414, May 28 2002

NYC 9/11 Public Portal Document LDLdLy DEdLCL COLLpOUIU RCDOL L

Data File : C:\MSDCHEM\1\DATA\051702\11413.D Vial: 22 Acq On : 18 May 2002 6:43 am Operator: Mclean Sample : 5/15 eh Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L

Peak Number 5 Phenanthrene, 2-methyl- Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T.

22.58 0.29 ug/L 389107 Phenanthranene - dl 0 22.95

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Phenanthrene, 2-methyl- 192 C15H12 002531-84-2 53 2 Phenanthrene, 1-methyl- 192 C15H12 000832-69-9 53 3 Phenanthrene, 9-methyl- 192 C15H12 000883-20-5 50 4 1,5-Naphthalenedithiole 192 C10H8S2 1000223-69-5 45 Abundance Scan 3319 (22,580 min): 11413.D (-3307) (-) m/z 192.10 fl ioo.oo%| 192

..... A... A 5000

42 54 7P 0 । 96 I 118 146 160 22.20 22.40 22.60 22.80 23.00 0 '1 | i i 1 1 । 1 i । 1 [ H f 1 j > I 1 i । in I 1 | 1 1 I I j I I i 1 pt 11 i । 1 1 1 1 । । । । | [ । i 1 ------- Ir m/z 191.00 18.17% m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #125842: Phenanthrene, 2-methyl- 192

5000 22.20 22.40 22.60 22.80 23.00 m/z 146.00 14.32%

mz-> Abundance 0'| 27| 1 mt 39i i i I51 63 [ i i I | | i'i ' ‘ | 82 96 Il 115 126 139 152 165 176 j . — I | I । I ■ | 1 1 > ■ | ■ I r 1 Di i | I J I l'| I I I I ['I I I I | l'l | I | | ! |'I j ) | I’I’l 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 #125856: Phenanthrene, 1-methyl- u 192 00 y-1 22.20 22.40 22.60 22.80 23.00 5000 m/z 96.00 13.75%

27 39 51 63 82 96il E 178 115 126 139 152 195 । 0 ' r 1 ‘' i ■ ■ " i "' ■ i'"' i "i I'1 1 "E ' 1 । ' I ' " ' 1 1 ' " I ' I ' ' '”1 ' ' uttm) ''II l|H th I I I’I’ m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #81033: Phenanthrene, 9-methyl- 111111 1*41 - 147 TI8 192 22.20 22.40 22.60 22.80 23.00 m/z 193.10 13.16% A 5000

m/z~> o TI 29 39 51 63 74 83 i " " I " " I'' “ ITTTTTTTTTTWTTTHTT 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 96 il 115 126 139 152 4rs । 176 . mm 22.20 22.40 22.60 22.80 23.00

11413.D 050102.M Tue May 21 15:56:31 2002 Page 8

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