GC/MS analysis results for sample AE11414, May 28 2002

NYC 9/11 Public Portal Document DCaLA wULpuLL LPVL

Data File : C:\MSDCHEM\1\DATA\051702\11413.D Vial : 22 Acq On : 18 May 2002 6:43 am Operator: Mclean Sample : 5/15 eh Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST9 8.L * ******************************************************************** Peak Number 6 Phenanthrene-diO Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T.

23.11 0.43 ug/L 581572 Phenanthranene - dl 0 22.95

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Phenanthrene-diO 188 C14D10 001517-22-2 93 2 Anthracene-dlO- 188 C14D10 001719-06-8 93 3 Cycloheptanone, 4-phenyl- 188 C13H160 067688-28-2 50 4 2-Quinolinecarboxaldehyde , 8-hyd... 188 C10H8N2O2 005603-22-5 40 Abundance Scan 3409 (23.109 min): 11413.D (-3402) (-) m/z 188.10 100.00% 188

5000 ............... 80 94 iw 42 52 66 J 132 146 77 22.80 23.00 23.20 23.40

m/z-> 0 1J J 1 » I I I 1 1 1 I I I I I I "I’r I I I l' f I ■ । ■ 1111 ■ 1111 ■ i i | F | । । । । । । । t i । ■ । । । । 1 । । । p r-i 11 । < i I i। । : i । । । 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 km m/ Z 94.05 13.82% Abundance #79827: Phenanthrene-d10 188

,.................................. 5000 22.80 23.00 23.20 23.40 m/z 80.10 13.79% 80 94 160 30 42 52 66 1 108 118 132 146 1, 170179 0 TPWTTTWTUTTTTTTTTHTTTTTH । । 1 | I I । i p । I I | I । । J | I I । I | I 1 J I | । I I I | । !’tl" 1 । i | r i |Hl’t i i i it

mfe-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79826: Anthracene-d10- 188 mn 22.80 23.00 23.20 23.40 5000 m/z 189.20 12.83% A 80 94 160 _ 66 17 30 42 52 0 ' I ‘ " 111" ' 11" 111' " i111 plipal 108 118 132 I" " . . ........ TT 146.11.179179,.., m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79739: Cycloheptanone, 4-phenyl- US 22.80 23.00 23.20 23.40 117 104 m/z 184.10 11.17% 91 160 5000 131 170 27 39 51 65 78 145

m/z-> 0 r 11 l । Anpo ml i'i n 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 + I" " i ....................................... 22.80 23.00 23.20 23.40 ,

11413.D 050102.M Tue May 21 15:56:33 2002 Page 9

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