GCMS blank analysis results for sample AE06338, May 2 2002

Machine-extracted title · confidence 100%

Gas chromatography-mass spectrometry blank analysis showing results below method detection limits for organic compounds.

NYC-WTC_000044433–000044446

Folder label: “GCMS X 4/29/02 A 5/1/02”

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\MSDCHEM\1\DATA\050102\0429LB.D Vial: 10 Acq On 1 May 2002 5:02 pm Operator: Mclean Sample Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L

Peak Number 6 Anthracene-d10- Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

23.11 0.51 ug/L 298855 Phenanthranene -dl0 22.95

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Anthracene-d10- 188 C14D10 001719-06-8 9 2 Phenanthrene-diO 188 C14D10 . 001517-22-2 3 Pyrrolo[2,3-b]indole, 1,2,3,3a,8.. . 188 C12H16N2 004089-16-1 53 4 Benzene, 1-(1-cyclohexen-l-yl)-4... 188 C13H160 020758-60-5 52 Abundance Scan 3410 (23.115 min): 0429LB.D (-3404) (-) m/z 188.10 100.00% 188

5000

94 ........ /............................. 1 > । । । । । । । । । । । । i । i । i i 'i- r । 40 22.80 23.00 23.20 23.40 156 57 66 80 ....... .. ...... . Ji,...... . I | t i | i I I i | > i I I | I r i i | i i i । i i I । p i < i ] । । । । । > I I । । । I । । । i i r t । । i । । । । । । । । । I ri । । । m/ z 94.10 19.11% m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79826: Anthracene-d10- 188

5000 -- 22.80 23.00 23.20 23.40 m/z 40.10 14.20% 80 94 160 J. PMMAANv/w 66 17 30 42 52 'l I I I I I I I I I I I I I I I I I I > 1 I I I । । i I । । । । H+ | rm —108 118 132 I I I I I I I I I I I I I P I I I I I146 ' —+4179179— mlz-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79827: Phenanthrene-d10 188 । f । । i । । । । i m । i ■ । । । i i i i । 22.80 23.00 23.20 23.40 5000 m/ z 184.05 11.43%

80 94 160 ' 30 42 52 66 Iril, 11 I I I ■ 1 1 I I I I I I I I I I I I I II I I I i > I I I I I I I I r I 108 118 132 146 | L| 170179,1,1111 I 11 i | IITITTI m । । । । । । I i । । । । । । 11 । rl'l p । । । । । । < । 11 I 11 । iii> m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79762: Pyrrolo[2,3-b]indole, 1,2,3,3a,8,8a-hexahydro-3a,8... 11 — 1 144 188 22.80 23.00 23.20 23.40 m/ z 18 9.10 10.72% 158 5000

130 173 II 42.51. . 65, . 771.91.-193,-11Ra.p ------ 1‘1111‘11/11/11/1/1/+/d/I411I m/z--> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 22.80 23.00 23.20 23.40

0429LB.D 050102.M Thu May 02 14:53:47 2002 Page 9

NYC-WTC_000044444

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