NYC-WTC_000045643
Laboratory report detailing GC/MS analysis of sample AE10609 including surrogate recovery data in May 2002.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗Document / 23 pages
GCMS sample analysis results for AE10604, May 10 2002
Machine-extracted title · confidence 100%Laboratory report detailing GC/MS analysis of sample AE10604 including surrogate recovery data in May 2002.
NYC-WTC_000045595–000045617Folder label: “GCMS X 5/3/02 A 5/7/02”
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OCR text
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document Library Search Compound Report
Data File C:\MSDCHEM\1\DATA\050702\10604.D Vial: 9 Acq On 7 May 2002 7:39 pm Operator: Mclean Sample 5/3 kb Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e
Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L
Peak Number 8 Trisiloxane, 1,1,1,5,5,5 -he... Concentration Rank 7
R.T. EstConc Area Relative to ISTD R.T.
33.25 0.28 ug/L 227984 Perylene-dl2 34.71
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 Trisiloxane, 1,1,1,5,5,5-hexamet... 384 C12H3604Si5 003555-47-3 27/ 2 3,6-Dioxa-2,4,5,7-tetrasilaoctan... 294 C10H30O2S14 004342-25-0 25 3 Hexasiloxane, 1,1,3,3,5,5,7,7,9,... 430 C12H38O5S16 000995-82-4/16 4 2-(2,6,6-Trimethylcyclohex-l-eny. .. 222 C14H2202 1000185-64-1 12 Abundance Scan 5134 (33.244 min): 10604.D (-5126) (-) m/ z 73.10 100.00% 73
147 221 5000 281 355 A 1110A AA. 11,. ‘ ' I 1 1 * __ 429 33.00 33.20 33.40 33.60 ।_| I r _______ । _________ m/z 147.10 61.82% I ‘l T 1 1 1 1 1 I-1 > I I | I II |II
m/z-> 50 100 150 200 250 300 350 400 A Abundance #26961: Trisiloxane, 1,1,1,5,5,5-hexamethyl-3,3-bis[(trime... 73 147 281 5000 -A A.................... 1 ■ 1 1 1 1 1 1 r ■ 33.00 33.20 33.40 33.60 369 m/z 221.10 51.94% 45 207 20 310 341 | 1 ‘I |"| 226 i" 177 T‛1" 249 । rti। 95 117 m/z-> H 50 T-r-r-r-r- । 100 150 200 250 > 300 । । । । । 350 । । T‘ । । 400 । r
Abundance #87890: 3,6-Dioxa-2,4,5,7-tetrasilaoctane, 2,2,4,4,5,5,7,7... 147 221 ’ 1 I ' 1 1 1 1 1 1 1 ' I 1 ' 1 1 I ' ' 73 33.00 33.20 33.40 33.60 5000 m/z 281.10 33.29% 191 117 279 45 249 [ - TI 1 r 1" ' 1 1 ' t [—.■ . T 1 I r-T m/z-> Abundance 50
73 100 150 200 250 300 350 #27715: Hexasiloxane, 1,1,3,3,5,5,7,7,9,9,11,11-dodecamethyl- 400 A33.00 33.20 33.40 33.60 m/z 355.00 25.23%
5000 207 281 133 341 415
/z-> 44 50 103 100 ... {53 177 1 TLB 150 200 , 234253 1 1 '1 1 1 250 1 300 309 ′ . L | L . I I I | 41 350 rr— 400 ■ ■ 1 ■ ■ ■ > । 1 1 ' 1 ' 1 33.00 33.20 33.40 33.60 1 ■ 1 1 1
10604.D 050102 .M Thu May 09 09:08:34 2002 Page 11
NYC-WTC_000045610
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NYC-WTC_000045610Source: NYC Law Department, mirrored locally
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