NYC 9/11 Public Portal Document
Library Search Compound Report
Data File C:\MSDCHEM\l\DATA\050802\10305R.D Vial: 26
Acq On 9 May 2002 12:56 pm Operator: Mclean
Sample re-inj Inst Instrumen
Mise Multiplr: 1.00
MS Integration Params: LSCINT.e
Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator)
Title : 508 Modified GC/MS scan
Library : C:\DATABASE\NIST98.L
Peak Number 10 Trisiloxane, 1,1,1,5,5,5-he... Concentration Rank 15
R.T. EstConc Area Relative to ISTD R.T.
34.37 0.24 ug/L 184396 Perylene-dl2 34.70
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 Trisiloxane, 1,1,1,5,5,5-hexamet... 384 C12H3604Si5 003555-47-3 32
2 2-(2,6,6-Trimethylcyclohex-l-eny... 222 C14H22O2 1000185-64-1 22
3 Valeraldehyde, (o-nitrophenyl)hy... 221 C11H15N3O2 005977-70-8 9
4 .alpha.-Tetraloxime, 5,6-dimethoxy- 221 C12H15NO3 1000125-87-9 9
Abundance Scan 5325 (34.367 min): 10305R.D (-5316) (-) m/ z 73.10 100. 00%
73 221
147
5000 281
44
355 A AAAA MMMA4 A4. MiA/MaanNMAY
96 429 34.00 34.20 34.40 34.60 34.80
0- I T ' kL1 1—1 1 i 1 ‘ । i < r kit ' ■ 1 1 1 1 1 _L m/z 221.10 83.50%
m/z-> 50 100 150 200 250 300 350 400
Abundance #26961: Trisiloxane, 1,1,1,5,5,5-hexamethyl-3,3-bis[(trime...
73 147
281
5000
34.00 34.20 34.40 34.60 34.80
369
m/z 147.10 80.00%
45
0- ■ r ‘
95 117 | i 177,227226 2l9 i 1 [ .1 13101 1 13411 1 1|
1 1 1 1 1
m/z-> 50 100 150 200 250 300 350 400
Abundance #66034: 2-(2,6,6-Trimethylcyclohex-1 -enyl)cyclopropanecarb...
147
A
34.00 34.20 34.40 34.60 34.80
107
5000 175 207
m/z 281.10 44.39%
41 79
0- LQllh ,, ill. । ,1,1,
m/z-> 50 100 150 200 250 300 350 400
Abundance #126930: Valeraldehyde, (o-nitrophenyl)hydrazone
211 34.00 34.20 34.40 34.60 34.80
77
52
m/z 355.10 28.90%
5000
161
104 135
0
L I 11 k l 4 d i | , 186
' 1 ' i 1 1 1 1 ' 1 1 1 1 1 ■ ' 1 1 1 ' ' 1 1
m/z-> 50 100 150 200 250 300 350 400 34.00 34.20 34.40 34.60 34.80
10305R.D 050102.M Thu May 09 13:51:07 2002 Page 13
NYC-WTC_000045130
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