NYC-WTC_000045643
Laboratory report detailing GC/MS analysis of sample AE10609 including surrogate recovery data in May 2002.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗Document / 23 pages
GCMS sample analysis results for AE10604, May 10 2002
Machine-extracted title · confidence 100%Laboratory report detailing GC/MS analysis of sample AE10604 including surrogate recovery data in May 2002.
NYC-WTC_000045595–000045617Folder label: “GCMS X 5/3/02 A 5/7/02”
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OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document Library Search Compound Report
Data File C:\MSDCHEM\1\DATA\050702\10604.D Vial: 9 Acq On 7 May 2002 7:39 pm Operator: Mclean Sample 5/3 kb Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 13 Trisiloxane, 1,1,1,5,5,5-he... Concentration Rank 10
R.T. EstConc Area Relative to ISTD R.T. 37.79 0.26 ug/L 215979 Perylene-dl2 34.71 Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 Trisiloxane, 1,1,1,5,5,5-hexamet... 384 C12H3604Si5 003555-47-3 43 2 3,6-Dioxa-2,4,5,7-tetrasilaoctan. . . 294 C10H3002Si4 004342-25-0 38 3 1-Monolinoleoylglycerol trimethy... 498 C27H54O4Si2 054284-45-6 33 4 3-Isopropoxy-1,1,1,7,7,7-hexamet. . . 576 C18H5207Si7 071579-69-6/28 Abundance Scan 5907 (37.786 min): 10604.D (-5896) (-) m/ z 73.05 100.00% 73 147 221
5000
191 281 355 429 Mulhm tte 40 96 1........... "I f ' 1 1 I ' 11 1. 1 f p1 r 1 1 | 1 ’11 * ’’I* Tin 37.40 37.60 37.80 38.00 38.20 m/ z 147.00 85.53% m/z--> 50 100 150 200 250 300 350 400 450 Abundance #115144: Trisiloxane, 1,1,1,5,5,5-hexamethyl-3,3-bis[(trim... 73 147 ............/.................... 5000 I-1 k I I I r I I ‘ [ TdB/n/d/kB.
281 37.40 37.60 37.80 38.00 38.20 m/z 221.00 71.78% 45 369 ' i ' 117 207 ■ 1 1 1 1 1 i ■ 1 —'l 1'1 11 1 1 249 1 1 1 ' m/z-> 50 100 150 200 250 300 350 400 450 Abundance #87890: 3,6-Dioxa-2,4,5,7-tetrasilaoctane, 2,2,4,4,5,5,7,7... 147 221
73 37.40 37.60 37.80 38.00 38.20 5000 m/z 355.10 35.78% 191 117 279 45 [ L 249 [ T— V' ' 1 1 1 r ”i-r “I| 1' r T r | i i “' 1 “ 1 । | 1 1 1 | I I I | | I
m/z-> 50 100 150 200 250 300 350 400 450 Abundance #27370:1-Monolinoleoylglycerol trimethylsilyl ether ' i 1 ‘ ■ 1 1 ‘ 1 ■ 1 1 1 1 1 ' 1 1 1 1 1 1 1 1 73 37 40 37.60 37.80 38.00 38.20 m/z 207.00 27.27%
5000 147 207 MapywwvNWwkooinaws 34 103 281 4 2.4412k . 177l ill 249 „ | 305327 355 325, 429 483 Pn 11.1 m/z-> 50 100 150 200 250 300 350 400 450 37.40 37.60 37.80 38.00 38.20
10604.D 050102.M Thu May 09 09:08:51 2002 Page 16
NYC-WTC_000045615
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