Laboratory report showing GCMS analysis results for sample AE12534 including surrogate recovery data on June 10, 2002.
NYC-WTC_000014578–000014606Folder label: “GCMS X 5/28/02 A 5/29/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\MSDCHEM\1\DATA\052902\12534.D Vial: 25 Acq On : 30 May 2002 5:37 am Operator: McLean Sample : gc/ms scan 5/28 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\052202.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 18 3,6-Dioxa-2,4,5,7-tetrasila. .. Concentration Rank 8
R.T. EstConc Area Relative to ISTD R.T.
36.43 1.28 ug/L 564858 Perylene-dl2 34.65 Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 3,6-Dioxa-2,4,5,7-tetrasilaoctan... 294 C10H3002Si4 004342-25-0 42 2 3-Isopropoxy-1,1,1,7,7,7-hexamet... 576 C18H5207Si7 071579-69-6 32 3 Trisiloxane, 1,1,1,5,5,5-hexamet... 384 C12H3604Si5 003555-47-3 27 4 Trisiloxane, 1,1,1,5,5,5-hexamet... 384 C12H3604Si5 003555-47-3 27 Abundance Scan 5677 (36.435 min): 12534.D (-5661) (-) m/ z 73.05 100.00% 73 147 221
5000 281 355 429 AMyrYy—MMY7 191 1 401 I 36.20 36.40 36.60 36.80
miz-> O+ I ’ 1 I ' ‘ ‘ * I ‘ ‘ 50 100 I ‘ 1 * 150 — 200 011277,1 250 300 350 --PP 400 450 500 550 m/z 147.10 93.58% Abundance #87890:3,6-Dioxa-2,4,5,7-tetrasilaoctane) 2,2,4,4,5,5,7,7... 147 2.11
73 5000 A... AA, * 36.20 36.40 36.60 36.80 191 m/z 221.10 76.12%
ti/z-> OPr 45 50 A .-* ,249.4 . 117
100 279
150 200 250 300 350 ‘ 460 ' 450 ' ‘ 500 ' 550 ‘ Abundance #26784:3-Isopropoxy-1,1,1,7,7,7-hexamethy!-3,5,5-tris(tri... 73
36.20 36.40 36.60 36.80 5000 m/z 355.00 35.04% 147 43 221 281 ' Pi i 1 327,.... 415........ .519 561 ’ 1*111 * 41**1*’ ’/*1 * mlz-> 50 100 150 200 250 300 350 400 450 500 550 .............. .... .................... Abundance #115144: Trisiloxane, 1,1,1,5,5,5-hexamethy1-3,3-bis[(trim... 73 36.20 36.40 36.60 36.80 147 m/z 281.00 32.14% __ 5000 281 45 369
n/z—> Of— 50 117 100 207 249 -------I- 150 200 250 300 350 400 450 500 550 MNAMWMM 36.20 36.40 36.60 36.80
12534.D 052202.M Mon Jun 03 11:46:58 2002 Page 21
NYC-WTC_000014603
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NYC-WTC_000012908
Laboratory report presenting analytical results for target compounds and surrogate recovery data for water sample AE11903.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000012937
Laboratory report presenting analytical results for target compounds and surrogate recovery data for water sample AE11904.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000013496
Laboratory report documenting GCMS analysis of sample AE11928 conducted on June 4, 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000014532
Gas chromatography-mass spectrometry analysis of sample AE12532 performed on 6/10/02, detecting 2,4-DDD surrogate at 77% recovery.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000014460
Laboratory report showing GCMS analysis results for sample AE12478 including surrogate recovery data on June 10, 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000012794
Laboratory report presenting analytical results for target compounds and surrogate recovery data for water sample AE11799.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000012989
Laboratory report presenting analytical results for target compounds and surrogate recovery data for water sample AE11907.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000014433
Laboratory report showing GCMS analysis results for sample AE12477 including surrogate recovery data on June 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000012852
Laboratory report presenting analytical results for target compounds and surrogate recovery data for water sample AE11901.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000012823
Laboratory report presenting analytical results for target compounds and surrogate recovery data for water sample AE11800.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000013014
GCMS laboratory report for sample AE11908 detecting unknown compounds and 2,4-DDD on June 4, 2002.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000022857
GCMS analytical report for environmental sample AE09155 including surrogate compound data from May 15, 2002.
1 shared topics · similarity 0.996
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NYC-WTC_000014348
DEP document containing gas chromatography-mass spectrometry data from late May 2002.
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Document page referencing GCMS methods and sample identification number NYC-WTC_000014348 dated May 28, 2002.
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Laboratory report showing GCMS blank analysis results for volatile organic compounds in sample AE12326 on June 3, 2002.
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Laboratory report showing GCMS calibration data for volatile organic compounds in sample AE12326 on June 3, 2002.
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Laboratory report showing GCMS reference analysis data for volatile organic compounds in sample AE12326 on June 4, 2002.
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