GCMS sample analysis results for AE10604, May 10 2002

NYC 9/11 Public Portal Document Library Search Compound Report

Data File C:\MSDCHEM\1\DATA\050702\10604.D Vial: 9 Acq On 7 May 2002 7:39 pm Operator: Mclean Sample 5/3 kb Inst : Instrumen Mise : Muitiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L

Peak Number 5 Noradrenaline tetraTMS Concentration Rank 8

R.T. EstConc Area Relative to ISTD R.T.

20.69 0.27 ug/L 338289 Acenapthalene-dlO 18.57

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Noradrenaline tetraTMS 457 C20H43NO3Si4 068595-65-3 32 2 N-(Trifluoroacetyl)-N,O,O',O''-t... 553 C22H42F3NO4Si4 1000072-26-7 23 3 Phenethylamine, N-methyl-.beta.,... 399 C18H37NO3Si3 010538-85-9 /23 4 N-Methyladrenaline, tri-TMS 413 C19H39NO3Si3 1000071-72-1 23 Abundance Scan 2997 (20.688 min): 10604.D (-2987) (-) m/ z 73.10 100.00% 73

5000 147 355 221 ................... .................. 281 Til [ । । ' I _|' i i rm । i i i k i r

401 20.40 20.60 20.80 21.00 45 327 ............................ L(,, 11 I 11— 1 ‘i 4 r i । [ I । । । 1 I I I I [ l i । r । । । । ' 177 f —I ‘ 1—I l l—J k I [ m/z 147.10 37.12% m/z-> 50 100 150 200 300 250350 400 450 500 550 Abundance #27959: Noradrenaline tetraTMS 73

5000 102 355 T i | I I Til | 3 1 । | । । r । । । r

20.40 20.60 20.80 21.00 m/z 355.00 33.60% 45 147 442 I ' ' I 1 ' 1 ‘ r ' ' I I | I I I I [ I I-1 I [ Illi | I I I-1 | । । r i T I I I I I I I I I I I I I I I

m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #27961: N-(Trifluoroacetyl)-N,O,O',O"-tetrakis(trimethyls... 73

355 20.40 20.60 20.80 21.00 5000 m/z 221.10 26.97%

45 | 116 147 193 236 267 ......................................... 538 1 1 i 1 m/z->______ 50 100 150 200 250 300 350 400 450 500 550 Abundance #115313: Phenethylamine, N-methyl-.beta.,3,4-tris(trimethy... i i | I I I I | r i । i 1l i i i | | I 73 20.40 20.60 20.80 21.00 m/ Z 281.00 18.87%

5000 355 44 116 147 193220 267 294 384 m/z-> dr* 1 t i | I I i i | iii , | i , i t । i r

50 100 150 200 250 300 350 400 450 500 550 20.40 20.60 20.80 21.00

10604.D 050102.M Thu May 09 09:08:23 2002 Page 8

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