NYC-WTC_000045643
Laboratory report detailing GC/MS analysis of sample AE10609 including surrogate recovery data in May 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗Document / 20 pages
GCMS analysis results for sample AE10610, May 10 2002
Machine-extracted title · confidence 100%Laboratory report detailing GC/MS analysis of sample AE10610 including surrogate recovery data in May 2002.
NYC-WTC_000045662–000045681Folder label: “GCMS X 5/3/02 A 5/7/02”
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OCR text
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document Library Search Compound Report
Data File C:\MSDCHEM\l\DATA\050702\10610.D Vial: 13 Acq On 7 May 2002 10:55 pm Operator: Mclean Sample 5/3 kb Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.e
Quant Method : C:\MSDCHEM\l\METHQDS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L Peak Number 3 N-(Trifluoracetyl)-O,O',O''. Concentration Rank 9 R.T. EstConc Area Relative to ISTD R.T.
20.69 0.21 ug/L 259870 Acenapthalene-dlO 18.57
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 N-(Trifluoracetyl)-0,O',O''-tris... 495 C20H36F3NO4Si3 054135-51-2 25 2 Benzoic acid, 2,4-bis[(trimethyl... 370 C16H30O4Si3 010586-16-0 25 3 Benzoic acid, 2,5-bis(trimethyls... 370 C16H30O4Si3 003618-20-0 XI 4 Phenethylamine, N-methyl-.beta.. 399 C18H37NO3Si3 010538-85-9/16 Abundance Scan 2997 (20.688 min): 10610.D (-2986) (-) m/z 73.10 100.00% 73
5000 355 147 221 281 1 i 1 ' 401 20.40 20.60 20.80 21.00 r 45 TI ............. 1 327 > । k k q kil I 1; 1 T I I | i i i i | ! i i ................................ ■ i • ■ ■ ■ i ■ ■ । • i > > ■ ■ । ■ m/z 355.10 45.57% m/z-> 0 50 100 150 200 250 300 350 400 450 500 Abundance #27963: N-(Trifluoracetyl)-O,O',O"-tris(trimethylsilyl)ep. .. 73 355
5000 20.40 20.60 20.80 21.00 m/z 147.10 37.09%| 45 1 h 110 140 184207 251 281 i । । ii i l ‘ । । < 1 r । ■ < । । । | । " । r । । । r । । । । r 324 1 I I “l“ I I I I 480 I I I I I
m/z-> 0 50 100 150 200 250 300 350 400 450 500 Abundance #115312: Benzoic acid, 2,4-bis[(trimethylsilyl)oxy]-, trim... 73
20.40 20.60 20.80 21.00 5000 355 m/z 221.10 33.15% 45
16 , , 105 133,163 193 223 251 ,281 321 I ' 1 ' 'l * r t' 1 ] ' I I ' I I I I I " [ I I ' I [ 1 l I I I I I 1 I I I I I I I I I I I I I I I m/z-> 0 50 100 150 200 250 300 350 400 450 500 Abundance #115317: Benzoic acid, 2,5-bis(trimethylsiloxy)-, trimethy... 7)3 20.40 20.60 20.80 21.00 355 m/z 281.10 19.14% 5000
45 15 147 179 223 I 267 297 1 105 J . l ’’ I 1 ’ "U’ uii ji l . . । i i—r । । । । t । । । a, ■ ■ ' i 1 1 TTET m/z-> 0 50 100 150 200 250 300 350 400 450 500 20.40 20.60 20.80 21.00
10610.D 050102.M Thu May 09 09:15:17 2002 Page 6
NYC-WTC_000045672
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NYC-WTC_000045672Source: NYC Law Department, mirrored locally
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