GCMS analysis report sample AE09677, May 23, 2002

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Library Search Compound Report Data File : C:\MSDCHEM\l\DATA\052102\9677.D Vial: 15 Acq On : 22 May 2002 12:44 am Operator: Mclean Sample : re-extract Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\052202.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 14 Trisiloxane, 1,1,1,5,5,5-he... Concentration Rank 16 R.T. EstConc Area Relative to ISTD R.T. 32.00 0.46 ug/L 404330 Chrysene-dl2 30.76 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Trisiloxane, 1,1,1,5,5,5-hexamet... 384 C12H3604Si5 003555-47-3 37 2 3,6-Dioxa-2,4,5,7-tetrasilaoctan... 294 C10H30O2S14 004342-25-0 32 3 Trisiloxane, 1,1,1,5,5,5-hexamet... 384 C12H3604Si5 003555-47-3 25 4 1H-Isoindole-1,3(2H)-dione 147 C8H5NO2 000085-41-6/12 Abundance Scan 4922 (31.999 min): 9677.D (-4911) (-) m/z 73.10 100/00% 73 147 221 5000- 281 355 429 31.60 31.80 32.00 32.20 32.40 191 0- —4? 50 100 150 1 ill ’ I ‘ ________ ‘ ‘ * I ‘ 44 1 | 1, 1 — m/z 147.10 74.11% niz-> 200 250 300 350 400 Abundance #26961: Trisiloxane, 1,1,1,5,5,5-hexamethyl-3,3-bis[(trime... 73 147 281 ----- 5000 31.60 31.80 32.00 32.20 32.40 369 m/z 221.10 58.22% 45 0- 4 i 95 117 1rei177 T f 207226 r-m-rin249, 310 341). r' r 1 ‘ I miz-> 50 100 150 200 250 300 350 400 Abundance #87890:3,6-Dioxa-2,4,5,7-tetrasilaoctane, 2,2,4,4.5,5,7,7... 147 2!1 ———....... 111

73 31.60 31.80 32.00 32.20 32.40 5000 m/z 281.00 38.12% 191

miz-> 0- 45 ■ 1 50 100 L +29 - 117

150 200 250 300 279

350 400 Abundance #115144: Trisiloxane, 1,1,1,5,5,5-hexamethyl-3,3-bis[(trim... 1 ■ ■ ■ ■ i ■ • ----- 73 31.60 31.80 32.00 32.20 32.40 147 m/z 355.10 33.56%

5000 281 45 369

miz—> 0 j__ 1 Lt 50 100 117 t 150 207 200 249 , 250 p 300 350 400 31.60 31.80 32.00 32.20 32.40

9677.D 052202.M Wed May 22 11:34:27 2002 Page 17

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