GCMS analysis results for sample AE06339, May 3 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\MSDCHEM\1\DATA\050102\6339.D Vial: 15 Acq On 1 May 2002 9:06 pm Operator: Mclean Sample re-ext 4/29 Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\l\METHQDS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 8 Phenanthrene-diO Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

23.11 0.60 ug/L 609380 Phenanthranene-dl0 22.96

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Phenanthrene-diO 188 C14D10 001517-22-2 93—) 2 Anthracene-diO- 188 C14D10 001719-06-8 87 / 3 Indolin-2-one, 3,3-di-t-butyl-l-... 259 C17H25NO 1000164-65-6 42 4 2-Quinolinecarboxaldehyde , 8-hyd... 188 C10H8N2O2 005603-22-5 40 Abundance Scan 3409 (23.109 min): 6339.D (-3401) (-) m/z 188.10 100.00% 188

5000 T I | I — I J ! n ! | I I I I | I — I r

80 94 160 22.80 23.00 23.20 23.40

m/z-> ....... 43 ... il.,. 20 40 60 80 100 120 140 160 180 200 220 240 268 260 ■ । ■ ■ ■ ■ । ■ i ■ < ■ m/ z 94.10 14.97% Abundance #79827: Phenanthrene-d10 188

5000 -- 22.80 23.00 23.20 23.40 m/z 189.10 13.90% 80) 94 160 _ 28 40 52 66 1, 11 i" 1 n i [ i i 11 । 1 r । l Il “108120132 1 | I i ' I ) 1 I' 1 I ' I■ 146I ill ■ k i i . |' )' ‘I I| >' I । । '1 I' | I । । I I I | । i । । 1 I I I । [7

m/z-> 20 40 60 80) 100 120 140 160 180 200 220 240 260 Abundance #79826: Anthracene-d10- 188 .umni rr । । । । । । । । । 22.80 23.00 23.20 23.40 5000 m/z 80.10 12.71%

80 94 160 28 40 52 66I 1 .' 1 .11, |106118 132 146 1 I | । । ■ r ■ ■1 ■ । T ■I i I I • I t■i I I■ I I■ I 1 rl I I m I I I I r I I I I ! IH" I > I I I I

ti/z->20 40 60 80 100 120 140 160 180 200 220 240 260 Abundance #79854: lndolin-2-one, 3,3-di-t-butyl-1-methyl- 188 a 22.80 23.00 23.20 23.40 m/ z 184.05 12.61%

5000 203 57 41 1 27 . 77 91 103115128 147 160172 I I III I I I I > r I I I । I1, । । i"1' ■ । । 'i । । 41 । r‘i । ।। h । । I11,। । । ■ i i । I ,| i i i | n i 239 । 259 | । । । | । । । । T I | I I । I [ I f T I ] I I I I | I I I I |" n/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 22.80 23.00 23.20 23.40

6339.D 050102.M Thu May 02 12:24:38 2002 Page 11

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