GCMS analysis results for sample AE06339, May 3 2002

NYC 9/11 Public Portal Document

Library Search Compound Report Data File C: \MSDCHEM\1\DATA\050102\6339.D Vial : 15 Acq On 1 May 2002 9:06 pm Operator: Mclean Sample re-ext 4/29 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title 508 Modified GC/MS scan Library C:\DATABASE\NIST98.L Peak Number 7 3-(2-Methoxy-5-methylphenyl... Concentration Rank 6 R.T. EstConc Area Relative to ISTD R.T.

22.58 0.35 ug/L 355081 Phenanthranene-dl0 22.96

Hit# of 5 Tentative ID MW MolForm CAS# Qua

1 3-(2-Methoxy-5-methylphenyl)acry... 192 C11H1203 103986-76-1 53 2 2-Propenal, 3-(3,4-dimethoxyphen... 192 C11H1203 004497-40-9 42 3 2-Imidazolidinone, 1-methoxy-3-p... 192 C10H12N2O2 052420-43-6 38 4 Anthracene, 9-methyl- 192 C15H12 000779-02-2 36 Abundance Scan 3319 (22.580 min): 6339. D (-3310) (-) m/z 192.10 100.00% 192

5000

40 70 82 ?f 146 160 22.20 22.40 22.60 22.80 23.00 THm+ 111" ■।111 ■ । ■ ■■ ■ । ■ —118 H mmmmmmm m/z 191.10 18.66% m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #80954: 3-(2-Methoxy-5-methylphenyl)acrylic acid 161 192

5000 105 1 i 1 1 22.20 22.40 22.60 22.80 23.00 77 132 91 m/Z 146.10 14.60% 115 145 .

/z—> --- 39 51 65 4 —23. 1,175. . I I I I I 1 I rI I I I I I I

20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #80953: 2-Propenal, 3-(3,4-dimethoxyphenyl)- 192 161 . ..... ...4..... .4 22.20 22.40 22.60 22.80 23.00 5000 m/z 96.10 13.59% 77 91 177 . 103 121। 138 149 । 52 64 ।'1 * 'T' 1 -I, I II r ri'! 1 mmel 1 , । h. I.. I I ■ ■ I I I I I I I I I I I I I I I I I I I I I I I I I I i I I I I I I I I I I 1 I I I I ‘III n/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #80907: 2-Imidazolidinone, 1 -methoxy-3-phenyl- 1 1 I 1 1 f I ’ 106 192 22.20 22.40 22.60 22.80 23.00 m/z 193.10 11.33%

5000 77 119 162 1 42 56 91

/z-> 28 4 U-+ I 64 I'' 1' r 11''11' " 11 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 TT 134 THT ■ I 1 ' 1.......... | I I I

22.20 22.40 22.60 22.80 23.00 I_I I I I I I I I I I

6339.D 050102.M Thu May 02 12:24:35 2002 Page 10

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