GCMS analysis results, sample AE09967, May 2002

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Library Search Compound Report

Data File C:\MSDCHEM\1\DATA\050602\9967.D Vial: 23 Acq On 7 May 2002 5:37 am Operator: Mclean Sample 4/25 Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L Peak Number 6 Ethanol, 2-(pentyloxy)-, ac.. Concentration Rank 8 R.T. EstConc Area Relative to ISTD R.T. 7.73 0.22 ug/L 170075 1,4-Diehlorobenzene-d4 9.94 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Ethanol, 2-(pentyloxy)-, acetate 174 C9H18O3 005312-09-4 10 2 3-Pyrrolidinol 87 C4H9NO 040499-83-0 9 3 Methyl 1-methylcyclopropyl ketone 98 C6H10O 001567-75-5 9 4 2-Propanone, 1-cyclopropyl- 98 C6H10O 004160/75-2 9 Abundance Scan 792 (7.733 min): 9967.D (-788) (-) m/ z 43.10 100.00% 43

5000

58 wwywo V ■ ■ । • ■ ■ , । । । ■ ■ , ■ । 87 98 7.40 7.60 7.80 8.00 ...........................1 1,1 +I— .. I....... ' l 1 ' 1 ' l ‘ 1 ' ' i 1 1 1 1 I ' ‘ ‘ 1 i 1 ' ■ ' i 1 1 1 1 1 1 > । m/ z 58.05 23.58% Tl/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #6217: Ethanol, 2-(pentyloxy)-, acetate 43

5000 WMMo 7.40 VA ' 1 i 1 1 1-1 1 1 1 ■' I 1 1 1 1 I 70 7.60 7.80 8.00 87 m/ z 87.10 14.46% ■■ । 29 556 I, - । 1 1 1,1 । । ll । । ।I III I I I I I T T-p-r 1 99 105 114 l 1 ' ' ' T' > ■ ■ । । 131 । ■ ■ ■ ■ । ■ ■ , ■ । m/z-> 10 20 30 40 50I 60 70 80 90 100 110 120 130 Abundance #4163: 3-Pyrrolidinol 43

7.40 7.60 7.80 8.00 5000 m/ z 59.20 13.30% 87 | 57 68

m/z-> ‘ 11’11’411111111 10 20 30 40 50 60 70 1,51ull,., Il 77,. ----- 80I 90 100 110 120 130 Abundance #5005: Methyl 1 -methylcyclopropyl ketone 43 7.40 7.60 7.80 8.00 m/z 41.20 11.66%

5000 55

<nlz-> 10 15 29 11111137/1 +11 20 30 49, । , 63 69 77 | 40 50 80 83 98 || । । । । । ' ' i ■ ' ■ 1 i ■ ■ ■ ■ i ■ ' ■ ' i ' ■ 1 ' i " " । 60 70 । । । । 90 100 110 120 130 IM __ 7.40 7.60 7.80 8.00 TTI

9967.D 050102.M Tue May 07 15:45:31 2002 Page 10

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