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GCMS analysis results, sample AE12533, June 2002

Machine-extracted title · confidence 100%

Laboratory report showing GCMS analysis results for sample AE12533 including surrogate recovery data on June 10, 2002.

NYC-WTC_000014552–000014577

Folder label: “GCMS X 5/28/02 A 5/29/02

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NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\MSDCHEM\1\DATA\052902\12533.D Vial: 24 Acq On : 30 May 2002 4:49 am Operator: McLean Sample : gc/ms scan 5/28 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\052202.M (Chemstation Integfator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L

Peak Number 17 Anthracene-dlO- Concentration Rank 15 R.T. EstConc Area Relative to ISTD R.T.

23.07 0.33 ug/L 395898 Phenant hranene - dl 0 22.91 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Anthracene-diO- 188 C14D10 001719-06-8 93 2 Phenanthrene-diO 188 C14D10 001517-22-2 93 3 Antipyrine 188 C11H12N20 000060-80-0 50 4 2-Quinolinecarboxaldehyde, 8-hyd... 188 C10H8N2O2 005603-22-5 42 Abundance Scan 3402 (23.068 min): 12533.D (-3395) (-) m/z 188.10 100.00% 188

5000

94 22.80 23.00 23.20 23.40 42 0-11— 66 80 . 160 m/z 94.10 15.24% mlz-> 10 20 30 40 50 60 70 80 90 100110 120 130 140 150 160 170 180 190 Abundance #79826: Anthracene-d10- 188

5000 22.80 23.00 23.20 23.40 m/z 189.15 13.93% 66। 80 94 160 , 17 30 42 52 J 108118 132 146 ,|.I 170179|,i 0 TWTTTTTTTT 1111111 11 11 111 i-| I h । [11 n 111111 ■ 1111111■ 111 r>1111'I'I'i ।ii 111111"‘l’tt iiii niz-> 10 20 30 40 50 60 70 80 90 100110120130140150160170180190 Abundance #79827: Phenanthrene-d10 188 - 22.80 23.00 23.20 23.40 5000 m/z 80.10 11.59%

80 94 160 30 42 52 66 . 11 108118 132 146 1I, 170179/1 I | > I 1 I | t I 1 I | I I I I | I I I 1 | ! I 1-1 I | I l t |TTfm 0 .| |

m/z-> 10 2030405060 70 8090 100110120130140150160170180190 Abundance #79725: Antipyrine 188 22.80 23.00 23.20 23.40 96 m/z 184.10 10.69%

5000 77 56 105 27 39 67 ! , | 115 130 145 159 173 || 0 । j i ■ 11111 i'i‘l. 11 r’Pi ■ 1t* । rpri n Hi ‘ l'| , Th | . ‘np . . rpr . . | 1 1'1 1 ‘ I I 1 1 | I1! 1 I | I I TTJVttt n/z-> 10 2030405060 70 8090 100110120130140150160 170 180 190 22.80 23.00 23.20 23.40

12533.D 052202.M Mon Jun 03 11:45:41 2002 Page 20

NYC-WTC_000014576

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NYC-WTC_000014576Source: NYC Law Department, mirrored locally

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