GCMS analysis results for sample AE11283, May 2002

NYC 9/11 Public Portal Document Llorary searcn compound Report

Data File : C:\MSDCHEM\1\DATA\020516\11283 .D Vial: 11 Acq On : 16 May 2002 7:15 pm Operator: Nefliu Sample : sample Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 ********************************************************************* Peak Number 2 Thiocyanic acid, 2-benzothi... Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 31.09 0.22 ug/1 15757 Phenanthrene-dl0 31.71 Hit# of 5 Tentative ID MW MolForm CAS# Qual

l Thiogyanic acid, 2-benzothiazoly. . . 192 C8H4N2S2 006011-99-0 42 2 2,4 (iH,3H)-Pteridinedione, 1,3-d... 192 C8H8N4O2 013401-18-8 40 3 1H-Indene, 2-phenyl- 192 C15H12 004505-48-0 36 4 2-Nitro-l-amino (5,6,7,8-tetrahyd. . . 192 C10H12N2O2 078422-66-9 9 Abundance Scan 4767 (31.088 min): 11283. D (-4759) (-) m/z 192.10 100.00% 192

5000 . .A 146 30.80 31.00 31.20 31.40 41 58 86 96 104 | 160 TTp—OOwg—HTTTTTTTTTTTTTTTTTTETTTTITTTTTT " i" m/z 191.10 16.74% m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #80870: Thiocyanic acid, 2-benzothiazolyl ester 192

5000 1 * r - ■ ■ ■ । ■ ■ i 1 ■ * ■ i * * 30.80 31.00 31.20 31.40 m/z 146.10 15.13% 45 1 T i , 90 , 108 122 134 148 160 J TmpmmmmmmmmmmmmmmmhPPP | " ■ I' ■ n/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #80889:2,4(1 H,3H)-Pteridinedione, 1,3-dimethyl- 80 19/2 ' 1 1 ‘ ‘ 1 ‘ I 1 ' ■ i ' 1 ■ ■ i 1 ■ 107 30.80 31.00 31.20 31.40 5000 27 135 m/z 193.20 9.78%

। 37 i| -- 55 TH Tpl i " " I " " 11' i " " i " " i'1 ‘' r " ■ i' ' i "' i" n/z-> Abundance 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 #125852:1 H-Indene, 2-pheny- 19/2 • 1 i ■ 1 ' ■ i 1 ■ I. 30,80 31.00 31.20 31,40 rn/z 160.20 8.70% 5000

27 39 51 63 74 83 96 115 126 139 152 165 176 ' ‘ I" " I'" 11' "' I " "! '■’ > h " 1 ’ I " “ I''111'1'' I 111' " I n ' ''111 " I'111111,1111 " 11111 ri' ■ ■ Il ’ 111’ ■ । • 1 1 ■ । 1 ■ m/z—> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 30.80 31.00 31.20 31.40

11283.D SCAN020507.M Fri May 17 13:03:25 2002 Page 4

NYC-WTC_000024572