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GCMS blank analysis report for sample AE12735, June 2002

Machine-extracted title · confidence 100%

Log sheet recording sample numbers, drip rates, pH levels, and other processing metrics for multiple environmental samples.

NYC-WTC_000015135–000015158

Folder label: “GCMS X 6/3/02 A 6/7/02

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Scanned page image, NYC-WTC_000015155
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NYC 9/11 Public Portal Document Llbrary searen compound keport

Data File C:\MSDCHEM\1\DATA\0 6 0 7 0 2\LBA.D Vial: 10 Acq On 7 Jun 2002 3:55 pm Operator: Sample gc/ms scan 6/3 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1\METHODS\060302.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 14 Thiocyanic acid, 2-benzothi... Concentration Rank 14 R.T. EstConc Area Relative to ISTD R.T.

22.53 0.25 ug/L 264227 Phenanthranene- dl 0 22.91 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Thiocyanic acid, 2-benzothiazoly... 192 C8H4N2S2 006011-99-0 53 2 5H-Dibenzo[a,d]cycloheptene 192 C15H12 000256-81-5 45 3 2-Propenal, 3-(3,4-dimethoxyphen... 192 C11H1203 004497-40-9/42 4 Phenanthrene, 9-methyl-_____________ 192 C15H12 000883-20-5 40 Abundance Scan 3311 (22.533 min): LBA. D (-3300) (-) m/z 192.10 1/00.00% 192

5000

— 82 96 146 160 22 20 22.40 22.60 22.80 42 51 #0 । । 0 TTTTmmmpmmmm Pr m/z 191.10 19.87% n/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #80870: Thiocyanic acid, 2-benzothiazolyl ester 1S2

5000 22.20 22.40 22.60 22.80 m/z 146.10 14.74% 0- — 45 — J 82 90 122! | 134 108 148 160 ..... — ■ | . 11" " | ■ t ■ ■ ■ ■ | ■ ■ ■ ■ | l'" . ■! 11 iz-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #80999:5H-Dibenzo[a,d]cycloheptene 192 -A ‘I * ‘ 1 ' 1 / k

22.20 22.40 22.60 22.80 177 5000 m/z 193.00 13.44% 89 165 39 51 I 63 76 97 115 128 139 152 0 TWTImTgmmhtTmp Hll ‘I1‘ niz-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #80953:2-Propenal, 3-(3,4-dimethoxyphenyl)- 192 22.20 22.40 22.60 22.80 161 m/z 160.10 11.14% 5000 77 121 149 177 91 103 52 64 138 0 - MH ■ r ' " i +] m/z—> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 22.20 22.40 22.60 22.80

LBA.D 060302.M Mon Jun 10 11:27:40 2002 Page 17

NYC-WTC_000015155

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NYC-WTC_000015155Source: NYC Law Department, mirrored locally

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