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GCMS analysis results for sample AE02787, March 11, 2002

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Laboratory report for DEP sample AE02787 showing unknown compounds and surrogate recovery data from March 11, 2002.

NYC-WTC_000005574–000005583

Folder label: “GCMS X 2/6/02 A 3/1/02

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NYC 9/11 Public Portal Document ulprary bearcr tompourd KEpOLL

Data File C:\HPCHEM\1\DATA\MAR0102\2787.D Vial: 21 Acq On 2 Mar 2002 4:01 am Operator: Sample gc/ms scan 2/6 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 Anthracene-dlO- Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

25.85 0.23 ug/1 23022 Phenanthrene-dl0 25.71

Hit# of 5 Tentative ID MW Mol Form' CAS# Qual 4-- *<------- 1 Anthracene -d10- / 188 C14D10 001719-06-8 64 2 4H-Pyrido [1, 2-a] pyrimidin-4-one, 3- 188 C11H12N2O 057773-19-0 40 3 Phenanthrene-diO 188 C14D10 001517-22-2 38 4 2-Quinoli Abundance Scan 2267 (25.852 min):8-hydrox carboxaldehyde, 2787.D (-) 188 C10H8N2O2 005603-22-5 9 | m/z 188.10..... 100.00% 188

5000- - 78 94 66 160 25.60 25.80 26.00 26.20 44 < 11 /1,»J ii ■ M THPT 7′17417 " i " " i'' ’ ’ r ’J' i ’'4 ’ i' j i ’ ’ * * i * Hm m/z 184.10 26.12%. m/z~> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 ; A Abundance #19957: Anthracene-d10- 188 ........... ..... I11

5000- 25.60 25.80 26.00 26.20 80 94 m/z 94.00 19.22%

80 904100 110 120 130 140 150 160 170 180— 66 160 . i ■ • ■ ■ । ■ i ■ > l ■ i' I 11111 i ■ ■'11 ■1 ■ ■ i1' ■' i m/z--> 40 50 60 70 190 Abundance 145 188 173 25.60 25.80 26.00 26.20 92 ' m/ Z 78.05 17.79% 5000 65 119 132 159 m/z-> _ 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #19958: Phenanthrene-d10 ,..... 108 25.60 25.80 26.00 26.20 m/z 189.05 10.46% 5000-

................................................. RA 80 94 160 , 1 "I" "I... .| 111...... ...... .......... I.. m/z-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 25.60 25.80 26.00 26.20 i

2787.D GCMS0208.M Tue Mar 05 10:52:49 2002 Page 2

NYC-WTC_000005582

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NYC-WTC_000005582Source: NYC Law Department, mirrored locally

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