GCMS analysis results for sample AE02787, March 11, 2002

NYC 9/11 Public Portal Document Library Search Compound Report

Data File C:\HPCHEM\1\DATA\MAR0102\2787.D Vial: 21 Acq On 2 Mar 2002 4:01 am Operator: Sample gc/ms scan 2/6 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 1 1,3-Dioxane Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

6.23 0.35 ug/1 25999 1,4-Dichlorobenzene-d4 12.31

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 1,3-Dioxafie 88 C4H802 000505-22-6 9 2 Ethane, isothiocyanato- 87 C3H5NS 000542-85-8 9 3 2-Propenenitrile, 2-chloro- 87 C3H2C1N 000920-37-6 9 4 Thiazolidine 89 C3H7NS 000504-78-9 9 Abundance Scan 130 (6.234 min): 2787.D (-) m/ Z 87.00.....100.00% 87 43 55 5000

71 103 -A-------- 5.80 6.00 6.20 W ' 6.40_ ____ 4449, ... ... INI i' ‘" i" " I ‘।' 111111'1 m/ Z 89.00 84.70% m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 Abundance #62909:1,3-Dioxane 87

5000 5.80 . hw . 6.00 6.20 6.40 6.60 31 58 m/ z 42.95 61.65% —A. TOu41—mUuu9CU—i, *mPCmCPm0n1p1mmT 11111101101101111111717 m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 Abundance ■ 87 59 .... ..AA. 5.80 6.00 6.20 6.40 6.60 5000 27 m/z 55.00 54.42% 72

34 46 1"' i"111'11 ■ i ■ ■ ■' i ■ ■" i'"11 ‘1 ‘ ■ i''" i' “11 ‘' i' “' i' • ■ ■ i " ■' i" " i ■" ■ i" " i1'" 1"111" " 111 m/z->....... ... 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 Abundance #740: 2-Propenenitrile, 2-chloro- 87 A...I, A ..... 5.80 6.00 6.20 a 6.40__ 6.60 m/z 40.95 21.99% 5000- 52

35 60 - Ti 47 1 । " ■ i1 ‘111" " i" " i ■' ■ ■ i" " i1111J " i" " 111" i"11111" i11" i" " i1 m 11"11"111" " ।" " i" | m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 5.80 6.00 6.20 6.40 6.60

2787.D GCMS0208.M Tue Mar 05 10:52:45 2002 Page 1

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