GCMS analysis results for sample AE10891, May 2002

NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\HPCHEM\1\DATA\MAY1502\10891.D Vial: 9 Acq On : 15 May 2002 9:54 pm Operator: Sample : GC/MS SCAN 5/10 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0510.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L Peak Number 2 1-Propene, 3-methoxy- Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 7.79 1.51 ug/1 93779 1,4-Dichlorobenzene-d4 12.16 Hit# of Tentative ID MW MolForm CAS# Qual

l 1-Propene, 3-methoxy- 72 C4H80 000627-40-7 36 2 3-Buten-2-one, 3-methyl- 84 C5H80 000814-78-8 32 3/3-Penten-2-one 84 C5H80 000625-33-2 17 4 (E)-l-Hydroxy-1,3-butadiene 70 C4H60 000000-00-0 17 Abundance Scan 300 (7.793 min): 10891 .D (-) m/z 41.05 100.00%| 41

5000 69

45 50 53 58 17 38 । 7.40 7.60 7.80 8.00 8.20 m/z-> mm +7---H2 84 TIPmmm m/z 43.05 69 57% 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 Abundance #62509:1-Propene, 3-methoxy- 4|1 72

45 5000 7.40 7.60 7.80 8.00 8.20 27 57 m/ z 69.05 44.95% 31 38 r i11111'1 *' i — " r ‘ " i " " i Hp miz-> 5 10 15 20 25 30 35 40 45 50 55 60 - 65 70 75 80 85 90 Abundance #62737:3-Buten-2-one, 3-methyl- 41 'I‘‘' T i M A* 7.40 7.60 7.80 8.00 8.20 5000 m/z 39.00 42.85% 69 84

38 44 50 ............... Tnu 1 ■ ■" i" ■ T 111 > 111111111.1111 TT4I... 11.. miz-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 Abundance #569:3-Penten-2-one —HTPT । 41 7.40 7.60 7.80 8.00 8.20 69 m/z 71.10 41.53% 5000 15 84 27 2/ 38 . 1 55 | ‘ 1 ' ' I ' ‘ ‘ I | i I I . । I I > . [J f ! . j l I I ( | | | I I | | | [ . JTI 1 rp i t i | I i I I । I I t i | J I I I | I'l I I | IT I I | I ) I I | J J I r | l t I 1.11 i i A । । । m/z—> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 7.40 7.60 7.80 8.00 8.20

10891.D GCMS0510.M Fri May 17 10:17:31 2002 Page 2

NYC-WTC_000024250