GCMS analysis results for sample AE04129, April 2002

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Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\MAR2202\4129.D Vial: 25 Acq On : 23 Mar 2002 7:44 pm Operator: Sample : gc/ms scan 2/25 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 Amylene Hydrate Concentration Rank 6

R.T. EstConc Area Relative to ISTD R.T.

7.30 0.64 ug/1 73587 1,4-Dichlorobenzene-d4 12.26

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Amylene Hyd: rate 88 C5H120 000075-85-4 39 2 3-Hydroxy-X~methyl-2-butanone 102 C5H10O2 000115-22-0 38 3 Propane, 2:-ethoxy-2-methyl- 102 C6H140 000637-92-3 36 4 3-Pentanol 88 C5H120 000584-02-1 3 6 Abundance Scan 245 (7.298 mln): 4129.D (-) m/z 59.05 100.00% 59

5000 43

107 ’Td*A**t***t*’’ITt14 38 1. 53 69 87 7.00 7.20 7.40 7.60 TTTTHhrndifiti hppmmptmp "i"' m/z 43.05 42.61% m/z~> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105110115 Abundance #62938: Amylene Hydrate 59

73 5000 43 31 7.00 7.20 7.40 7.60 m/z 107.00 17.37%

m/z-> 2s. d -rrn-r Inpgu IT I’’’’IE2-I—SLVTTTOOTOOTO’’ITTT 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105110 115 Abundance #1007 3-rdude • hLBtond 59

7.00 07.20 7.40 7.60 5000 43 m/z 41.05 17.25% 31 . 38 h ; 69 87 TTTpTTrjTTTTytTTTpTTTl+rrrpTrrpTrrpTTipTTTpTTTpTTTpTTTpT^ m/z--> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105110115 Abundance #63580: Propane, 2-ethoxy-2-methyl- 110T I* s s p amMA 10 1* 59 7.00 7.20 7.40 7.60 m/z 69.10 6.19% 5000 87 41 31 ...... I‘।M।1" I'''11 11 ‘ I' ■ ■' I' mr 1111111111111 > 11,11111111111u11h11>i.11>1111u1111111111111111 ... K... m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105110115 7.00 7.20 7.40 7.60

4129.D GCMS0308.M Wed Mar 27 10:06:18 2002 Page 2

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