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GC/MS analysis results for sample AD22754, Oct 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GC/MS analysis of sample AD22754 conducted on October 11, 2001, noting other unknown compounds.

NYC-WTC_000087403–000087416

Folder label: “GC/MS Scan 9/19/01

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Scanned page image, NYC-WTC_000087413
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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File ; C:\HPCHEM\l\DATA\SEP2801\22754.D Vial 19 Acq On : 29 Sep 2001 6:05 am Operator 10 9 GALOS Sample : gc/ms unknown I n .31 GC/MS 209 Mise Mui", iplr 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L *********************************************************^+:f t ********

Peak Number 3 3-Hexanol Concentration Rank 5 R.T. EstConc Area Relative to ISTD R. T . 6.62 0.44 ug/1 52259 1,4-Dichlorobenzene-d4 11 - ';'8 Hit# of 5. Tentative ID MW MolForm CAR# Qual 1 3-He^nol 102 C6H14O 010623-37-0 64 2 Amylene Hydrate 88 C5H12O 0C0075-85-4 38 3 Sjzlane, trimethyl- 74 C3H10Si 0C;0993-07-7 33 4 3^Pentanol 88 C5H12O 0(0584-02-1'33 Abundance Scan 172 (6.623 min): 22754.D (-) m/z 5 9.'5 10 0.00% 55 5(9

73 5000 41

670 0. rn 7,00 84 .......... Tm+p-rr m/z 5 5 7c ■’8 5.7 9% n/z~> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 Abundance #63528: 3-Hexanol 50 55

73 -----p]*’- 7- 1 r ■ 5000 31 __ 6.80 7.60 m/z 7 3'. (7o 54-82% 27 45 84 +b- ■*’1 • " ' I " " I H ■I Ti/z-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 Abundance #62940: Amylene Hydrate 50 6.20 6.40 7.00 _ 73 5000 45 m/z 41.15' 28.15% 55 31 27

5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 Abundance #62564; Silane, trimethyl- 5^ SAI ..5?’0 ,!’.O 7.00 m/’’. i' "T ■.■40%

5000 73

15 31 4245 11 ■ • ■ I"" I' i -111 ■" I"" I' I T‘''' I I'''' I'''' I ■n/z-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 6.20 6Aq, 6.60 6.80 7.00

22754.D NP091101.M Fri Oct 05 15:21:39 2001 Page 3 ‘ N YC-WTC_000087413“

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NYC-WTC_000087413Source: NYC Law Department, mirrored locally

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