GCMS analysis results for sample AE11602, June 2002

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\MAY2102\11602.D Vial: 31 Acq On : 22 May 2002 8:06 pm Operator: Sample : EXTRACTS/20 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0520 .M (RTE. Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 13 1-Hexanol, 5-methyl- Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T. 13.25 7.89 ug/1 506336 1,4-Dichlorobenzene-d4 12.15 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 1-Hexang1, 5 -methyl - 116 C7H160 000627-98-5 53 2 Acetic /acid, decyl ester 200 C12H2402 000112-17-4 38 3 1-Hexanol, 3-methyl- 116 C7H160 013231-81-7 38 4 2,4-p/methyl-1-heptene 126 C9H18 019549-87-2 36 Abundance Scan 896 (13.255 min): 11602.D (-) m/z 43.05 100.00% 43

5000 55 70 . . . — 61 83 98 13.00 13.20 13.40 13.60

mlz-> .... I, +49— 4— 20 30 40 50 60 70 80 90 115 125 100 110 120 130 '146 '156 143 m/z 55.10 44.64%

_A Abundance #3345:1-Hexanol, 5-methyl- 43 55 70

5000 ■ 13.00 13.20 13.40 13.60 31 m/z 70.05 42.20% 83 . I.... miz-> 20 30 40 50 60 70 80 90 100 110 120 130 ‘146 150 Abundance #22935: Acetic acid, decyl ester 43 A/ 13.00 13.20 13.40 13.60 5000 55 70 m/z 69.05 37.70% 61 83 9 112 niz-> 20 30 40 50 ‘ 1* ' 1 60 70 Igannam 1 1 1 1 1 1 ‘ i ■ 140 80 90 100 110 120 130 140 150 • i • • ■ ■ i ‘ ■»* [ • * • 11 ‘

Abundance #3374:1-Hexanol, 3-methyl- 43 55 13.00 ia20 13.40 13.60 70 m/z 56.10, 30.48%

5000 31

MMV./ 83 ' i 1 ■ ■ ■ i' '' ■ i r-r-p-r 1 . II...... 1...... 98................................ 1111 •T' • ‘ 1 I ’ ‘ * • 1 ’ • '' i • ’ * ‘ i ‘ ‘ ' i * ' ‘ * 1 ' 1 ‘ 1 1 1 ‘ 1 ‘ 1 1 TTT m/z—> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 13.00 13.20 13.40 13.60

11602.D GCMS0520.M Fri May 24 08:33:16 2002 Page 13

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