GCMS analysis results for sample AE11602, June 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\MAY2102\11602.D Vial: 31 Acq On : 22 May 2002 8:06 pm Operator: Sample : EXTRACTS/20 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P 2.r

Quant Method : C:\HPCHEM\1\METHODS\GCMS0520 .M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 12 Acetic acid, 2-ethylhexyl este Concentration Rank 5 R.T. EstConc Area Relative to- ISTD R.T. 13.15 4.03 ug/1 258852 1,4-Dichlorobenzene-d4 12.15 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Acetic acid, 2-ethylhexyl ester 172 C10H20O2 000103-09-3 33 2 1-Octene 112 C8H16 000111-66-0 28 3 2-Propenoic acid, 2-ethylhexyl este 184 C11H20O2 000103-11-7 28 4 2-Propenoic acid, 6-methylheptyl es 184 C11H20O2: 054774-91-3 25 Abundance Scan 885 (13.154 min): 11602.D (-) m/z 43.05 100.00% 43 55 70

5000

----- +4950— *60r- * 70L 61 83

■ ■ r-'''' i ■ ■ 98 । ■ - • • । - 115

' ' 1 1 1 1 1 1 1 1 _All 12.80 13.00 13.20 13.40 m/z 55.10 93.19% mfa-> 20 30 40 80 90 100 110 120 130 Abundance #15793: Acetic acid, 2-ethylhexyl ester

M.) 43

70 5000 TIur 57 12.80 13.00 13.20 13.40 83 m/z 70.15 69.37% 27 — 112 ■ ■ i • 1 1 '.'I.. L Ji t ,... 98........... [................. niz-> 20 30 40 50 ■ । - ■ 60 70 80 90 100 110 120 130 Abundance #2657:1-Octene 43 55 TP i 1 ■ 12.80 13.00 13.20 13.40 70 5000 m/z 56.10 26.43% 27 83

• ■ i - - I, i ■ IIH,L...... ..... ?7..... 112........... 1 I - - - • i ■ 1 - - i ■ 1 - - i - - ■ ■ i 1 ■ - - i ■ - ' ■ i ■ niz-> 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #68967:2-Propenoic acid, 2-ethylhexyl ester 1’1 55 12.80 13.00 13.20 13.40 m/z 41.15 25.00% 27 70 5000

mz—> ■ । 20 42 -1 • ■ - -11 - - -1 ■ ■ 30 40 50 60 70 1—80 i... 90 83

*4 100 124 110 120 130 112 , .. Tr AW 12.80 13.00 13.20 13.40

11602.D GCMS0520.M Fri May 24 08:33:15 2002 Page 12

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