NYC-WTC_000046249
Calibration table data for GCMS analysis of volatile organic compounds dated May 3-6, 2002.
1 shared topics · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗Document / 25 pages
GCMS analysis results for sample AE11602, June 2002
Machine-extracted title · confidence 90%TCLP calibration table document dated May 24, 2002, listing deuterated standards and response factors for GCMS analysis.
NYC-WTC_000013943–000013967Folder label: “GCMS X 5/24/02 A 5/28/02”
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NYC 9/11 Public Portal Document
Library Search Compound Report Data File : C:\HPCHEM\1\DATA\MAY2102\11602.D Vial: 31 Acq On : 22 May 2002 8:06 pm Operator: Sample : EXTRACTS/20 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C.\HPCHEM\1\METHODS\GCMS0520.M (RTE Integrator) "F Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 11 Acetic acid, hexyl ester Concentration Rank 9 R.T. EstConc Area Relative to. ISTD R.T. 13.11 1.97 ug/1 126541 1,4 -Dichlorobenzene-d4 12.15 Hit# of 5 'entative ID MW MolForm CAS# Qual 1 Acetic acid, hexyl ester 144 C8H1602 000142-92-7 36 2 1-Pentan 1, 2-methyl-, acetate 144 C8H1602 007789-99-3 25 3 Hexane, / , 11 -oxybis- 186 C12H260 000112-58-3 23 4 Pentanoic acid, 2,2-dimethyl-, ethe 156 C9H1602 044970-05-0 17 Abundance — Scan 880 (13.108 min): 11602.D (-) m/z 43.05 100.00%| 43
5000 56
- 70
m/z-> 10 1 * i *1 ■ ■ । ■1 * i * * * ′ 11 • i1 20 30 40 50 4 60 70 80 83 98 ng 90 100 110 120 130 140 150 12.80 13.00 13.20 13.40 m/z 56.10 49.03%| Abundance #66311: Acetic acid, hexyl ester 43
5000 56 12.80 13.00 13.20 13.40 m/z 41.05 17.95 15 27 1 I 69 , , ...... 84 ............................................. ... ...................... ‘ ■ i1 ■ ‘ ■ i ■ ’ ‘ ‘ i ■ ■' ■ i -n-p-r■ ■ i ■ ■ •* r* * ■ ■ ।11 ■ h ' ■ • * । * * * * ।1 * * * i * *1 * । •1 * * । * * * * i
_A miz-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 Abundance #8417:1-Pentanol, 2-methyl-, acetate 43 V 12.80 13.00 13.20 13.40 5000 m/z 70.15 14.84 56 84 30— 73 —— 101 144 tr 114 111'1111111111'1111'1' 11'1111 niz—s Abundance 10 20 30 40
43 50 60 70 80 90 100 110 120 130 140 150 #69125: Hexane, 1,1-oxybis- —MM. 12.80 13.00 13.20 13.40 85 m/z 57.10 13.08%
5000
/z-> 1aa/0mda/a009/0 10 20 27
30 40 56
PTTT II... 69.... 1’1111111-111111119221331311111133 50 60 70 80 90 100 110 120 130 140 150 _ ML 12.80 13.00 13.20 13.40
11602.D GCMS0520.M Fri May 24 08:33:14 2002 Page 11
NYC-WTC_000013958
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NYC-WTC_000013958Source: NYC Law Department, mirrored locally
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Laboratory report documenting GCMS analysis of sample AE11309 conducted on May 28, 2002, including surrogate recovery data.
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NYC-WTC_000046524
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Reviewed data file listing retention times and response factors for deuterated internal standards.
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NYC-WTC_000013913
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NYC-WTC_000013921
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