GCMS analysis results for sample AE11602, June 2002

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\MAY2102\11602.D Vial: 31 Acq On : 22 May 2002 8:06 pm Operator: Sample : EXTRACT5/20 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P 2**

Quant Method : C.\HPCHEM\1\METHODS\GCMS0520 .M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 10 1-Pentanol, 2-methyl- Concentration Rank 10 R.T. EstConc Area Relative to. ISTD R.T.

12.98 1.84 ug/1 117915 1,4-Dichlorobenzene-d4 12.15 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 1-Pentanol, 2-methyl- 102 C6H140 000105-30-6 36 2 3-Methylheptyl acetate 172 C10H20O2 072218-58-7 32 3 1-Butanol, 2-methyl-, acetate 130 C7H14O2 000624-41-9 28 4 Hexane,/ 3-methyl- 100 C7H16 000589-34-4 17 Abundance Scan 866 (12,980 min): 11602.D (-) m/z 43.05 100.00% 43

5000

56 70

,49/1161 .•g—aeT m/z70.15 II.i oc 85 98 । 105 AM W 12.60 12.80 13.00 13.20 13.40 29.74% ■'i 1 ' 1 ■ i ■ ■ • 1 i ■ • • ■ I* 11 - I ■ ' ‘ 1 i ' ‘ ■ ( miz- > 10 20 30 40 50 60 70 80 90 100 110 Abundance #63553: 1-Pentanol, 2-methyl- 43

5000 27 55 71 ■ । ■ •। ■ • AN 12.60 12.80 13.00 13.20 13.40 m/z 41.15 19.66% 84............................

miz-> 10 33 ■ i ■ ■ ■ ■ i ■ • ■ ■ i • ■ ' ■ i 20 30 40 *.. I... 50 60 7080 90 100 110 T

Abundance #15803:3-Methylheptyl acetate 40 _ Wy b 12.60 12.80 13.00 13.20 13.40 5000 70 m/z 56.10 19.30% 57 27 83 — ± 4 ---12. miz-> Abundance 10 20 30 40 50 60 70 80 #65217:1-Butanol, 2-methyl-, acetate 43 90 100 110 MV 12.60 12.80 13.00 13.20 13.40 m/z 69.05 18.85% 5000

_WN 70 15 27 55 I ■ ' i ■ ■ ■ ■ i ■ ■ ■ ■ i ■ t ,61 r 1 1 1 ,1 1 1I ' 1 ' I '_ --------- /z—> 10 20 30 40 50 60 70I 80 90 100 110 12.60 12.80 13.00 13.20 13.40

11602.D GCMS0520.M Fri May 24 08:33:13 2002 Page 10

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