NYC-WTC_000046249
Calibration table data for GCMS analysis of volatile organic compounds dated May 3-6, 2002.
1 shared topics · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗Document / 25 pages
GCMS analysis results for sample AE11602, June 2002
Machine-extracted title · confidence 90%TCLP calibration table document dated May 24, 2002, listing deuterated standards and response factors for GCMS analysis.
NYC-WTC_000013943–000013967Folder label: “GCMS X 5/24/02 A 5/28/02”
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NYC 9/11 Public Portal Document
Library Search Compound Report Data File : C:\HPCHEM\1\DATA\MAY2102\11602.D Vial: 31 Acq On : 22 May 2002 8:06 pm Operator: Sample : EXTRACTS/20 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0520 .M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 9 Acetic acid, decyl ester Concentration Rank 19
R.T. EstConc Area Relative to. ISTD R.T. 12.72 0.49 ug/1 31556 1,4-Dichlorobenzene-d4 12.15 Hit# of 5 -Tentative ID MW MolForm CAS# Qual
1 Acetic acid, decyl ester 200 C12H2402I 000112-17-4 28 2 Acetic acid, heptyl ester 158 C9H1802 000112-06-1 25 3 Acetic cid, butyl ester 116 C6H1202 000123-86-4 23 4 Ethyl . etate 88 C4H802 000141-78-6 12 Abundance Scan 838 (12.723 min): 11602.D (-) m/z 43.05 100.00% 43
5000 56 69 61 12.40 12.60 12.80 13.00 ' miz-> ' I ■' " I ' ■ ' 11+ 20 30 40 +51 50 LL 60 1 ■ i ■ 70 80 90 100 110 120 m/z 56.10 28.65% Abundance #69718: Acetic acid, decyl ester 43
5000 WA12.40 12.60 12.80 13.00 ‘ 27 56 70 m/ z 69.05 22.38% 61 Q2
m/z-> 20 30 40 T-r-J-r-r 50 60 • i ■ ■ 70 80 1-702—12—— 90 100 110 120 Abundance #11981: Acetic acid, heptyl ester 43 y_ /WAV 12.40 12.60 12.80 13.00 5000 m/z 55.10 19.29% 56 70 61 27 98 1. ii 89 | 116 tnlz-> 20 '30 ' ' 40 ' 'so’' 60 70 80 90 100 110 120 Abundance #64327: Acetic acid, butyl ester ■ • p '■ 43 12.40 12.60 12.80 13.00 m/z 41.15 17.99% 5000
m/z—> 27 ' I ‘ ‘ ' ‘ I ‘ ‘ 20 30 ‘ I ' 1
40 ‘ "T ‘ 50 56
4 60 61 73 1 87 ‘ ‘ I 1 ■ ‘ ■ i 1 ■ • ■ i ■ ■ ■ • i ■ ■ • ■ i ■ ■ ■ • i ■ • 70 80 90 100 110 120 —N 12.40 12.60 12.80 13.00
11602.D GCMS0520.M Fri May 24 08:33:13 2002 Page 9
NYC-WTC_000013956
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NYC-WTC_000013956Source: NYC Law Department, mirrored locally
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Calibration data for GCMS analysis of volatile organic compounds recorded on April 23, 2002.
1 shared topics · similarity 0.988
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Calibration data for GCMS analysis using 625/TCLP method with deuterated compound reference standards recorded on February 21, 2002.
1 shared topics · similarity 0.988
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000024997
Laboratory report documenting GCMS analysis of sample AE11309 conducted on May 28, 2002, including surrogate recovery data.
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