GCMS analysis results for sample AE11602, June 2002

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\MAY2102\11602.D Vial: 31 Acq On : 22 May 2002 8:06 pm Operator: Sample : EXTRACTS/20 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:.\HPCHEM\1\METHODS\GCMS0520 .M (RTE Integrator) -= Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 8 Acetic acid, hexyl ester Concentration Rank 17 R.T. EstConc Area Relative to ISTD R.T. 12.03 0.51 ug/1 32605 1,4-Dichlorobenzene-d4 12.15 Hit# Of 5 Tentative ID MW MolForm CAS# Qual 1 Acetic acid, hexyl ester 144 C8H16O2 000142-92-7 39 2 1-Hexanol 102 C6H140 000111-27-3 25 3 l-Pentene, 4-methyl- 84 C6H12 000691-37-2 9 4 Cyclopentane, methyl-__________ ____ 84 C6H12 000096-37-7 9 Abundance / Scan 762 (12.027 min): 11602.D (-) m/z 43.05 100.00% 43

56 5000 61 69 TTTT 84 11.60 11.80 12.00 12.20 12.40

m/z—> TWPPTOTTTTTTTTTT A+51 mm ।। n n p .Trp rrry 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 m/ z 56.10 50.75% Abundance #66310: Acetic acid, hexyl ester 43

5000 ~i 11 ■ n 1r’ IITITT1T 56 11.60 11.80 1200 1220 1240 61 m/z 61.15 38.24% 27 69 84 mmmmmmmmmm „ |....... | | ........ |........... 101....... m/z—> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 ’ Abundance #63563:1-Hexanol 56 i ' 1 ■ ■ i ■ ■ • • i • ■

43 11.60 11.80 12.00 1220 12.40 5000 m/z 42.15 27.05% 69 31 84 “ 11111 ‘ ‘ 1 ‘" I “ mmpmp H 1111.1.. 1. |. U111 n 111 ■ 11111 n (I n 1111 n I m/z—> Abundance 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 #599:1-Pentene, 4-methyl- 43 a.M.A M 11.60 11.80 12.00 12.20 12.40 m/z 55.10 25.81% 5000

m/z—> « 19 51 69 84 1 27

mTTTTHTTTmTTTTTm 56

5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 A 11.60 11.80 12.00 1220 12.40

11602.D GCMS0520.M Fri May 24 08:33:12 2002 Page 8

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