GCMS analysis results for sample AE11602, June 2002

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\MAY2102\11602.D Vial: 31 Acq On : 22 May 2002 8:06 pm Operator: Sample : EXTRACTS/20 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0520 .M (RTE Integrator) ** Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 7 Furan, 2,3-dihydro- Concentration Rank 14 R.T. EstConc Area Relative to ISTD R.T. 10.52 0.72 ug/1 45967 1,4-Dichlorobenzene-d4 12.15 Hit# Of 5 Tentative ID MW MolForm CAS# Qual 1 Furan, 2/3-dihydro- 70 C4H60 001191-99-7 64 2 2-Butenal, (E) - 70 C4H6O 000123-73-9 50 3 Butane/ 2-cyclopropyl- 98 C7H14 005750-02-7 28 4 Formic acid, pentyl ester 116 C6H1202 000638-49-3 28 Abundance 7 Scan 598 (10,524 min): 11602.D (-) m/z 70.05 100.00%

A 41 7)

5000 55 ‘ I ' ‘ ' I ‘ ‘ ‘ I ' ’ • ‘ I 14 T 45 10.20 10.40 10.60 10.80 58 67 -#11′1111-2011111012371103141. J........ 8386..... m/z 41.05 98.34% miz-s 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 Abundance #212: Furan, 2,3-dihydro- 70 41

5000 10.20 10.40 10.60 10.80 m/z 69.15 80.47% 27 38 44 49 55_______ , - -354 11*9 4 ■ i' ■ ■ ■ i ■' ■ ■ i ■ ■ ■ ■ i ■ nz-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 Abundance #62443:2-Butenal, (E)- 41 70 10.20 1040 10.80 lotA ' 27

A 5000 rn/z 55.10 40.76% 38

miz—s 20 25 ‘ 1411118 30 33 35 .48 .......... । 40 45 50 55 60 55 70 75 80 85 90 ।1" I1 “ 1111" i1"11111 ■ i

Abundance #1317: Butane, 2-cyclopropyl- 70 ...... M 55 10.20 10.40 10.60 10.80 41 m/z 56.10 38.04%

5000

27 51 67 mP ■ 11■■■i‘■■■।"831 ■ । । । r miz-s 20 25 ■' i “ ■ ■ i ■" ■ i 30 35 40 45 50 55 60 65 70 75 80 85 90 1 ■ i ■ ' ■ ‘ i 10.20 10.40 10.60 10.80

11602.D GCMS0520.M Fri May 24 08:33:11 2002 Page 7

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