GCMS sample analysis report for AD29927, Jan 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\DEC1401\29791A.D Vial: 47 Acq On : 16 Dec 2001 11:37 am Operator: 209 GALOS Sample : gems scan 12/11 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 Furan, 2,3-dihydro-4-methyl- Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

6.37 0.29 ug/1 70382 1,4-Dichlorobenzene-d4 11.68

Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 Furan, 2 ,/3 -dihydro-4-methyl - 84 C5H80 034314-83-5 58 2 2-Butenal, 3-methyl- 84 C5H80 000107-86-8 50 3 2-Butenal, 2-methyl- 84 C5H80 001115-11-3 43 4 2-Butenal, 2-methyl-, (E)- 84 C5H80 000497-03-0 38 Abundance Scan 144 (6.369 min): 29791A.D (-) m/z 83.95 100.00% 55 84

39 5000

69 103 6.00 6.20 6.40 6.60 6.80 r •" i1 • * • i TH + +HT 1IIWIPPWPWHITTTT m/z 55.0.0 83.70% m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 Abundance #557: Furan, 2,3-dihydro-4-methyl- 55 84

5000- 41 AAA 4 )44, ■ , —Ir < > । । > 14 fr 27 6.00 6.20 6.40 6.60 6.80 69 m/ z 83.0.5 55.71% 50 । « 11 ■ ■ > • । ■ ■ ■ > । I"” I । ■ ■■ ■ । ... H r "' I T’TTTT m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 Abundance #62726: 2-Butenal, 3-methyl- 84 -A,A-M-A— AAAMAMA 6.00 6.20 6.40 6.60 6.80 5000 41 55 m/ z 39.05 54.13%

50 t . 69 ‘ I‘B‘‘T"TIIIE‘I‘TTTTTT TI"n——n——mUBmgu rn/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 Abundance #62740: 2-Butenal, 2-methyl- M , yen 55 84 6.00 6.20 6.40 6.60 6.80 m/z 59.05 45.58% 5000 - 29

Tper —3744 54 - I ■ ■ ■ ■ i" " i" ■' i'" ■ i ■ ■ ■ ■ i'1 A l T TT*. | PI V I | I I T I | 1 I I f I1 1 m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 6.00 6.20 6.40 6.60 6.80

29791A.D GCMS1126.M Wed Jan 30 11:49:24 2002 Page 1

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