GCMS analysis report for sample AE01040, Feb 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\FEB1102\1040.D Vial: 28 Acq On : 12 Feb 2002 12:27 pm Operator: 209 GALOS Sample : GC/MS SCAN 1/15 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 2-Butenal, 2-methyl- Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

6.94 0.31 ug/1 31361 1,4-Dichlorobenzene-d4 12.35

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Butenal, 2-methyl- 84 C5H80 001115-11-3 64 2 2-Pentyn-I-ol 84 C5H80 006261-22-9 59 3 2-Ethylacrolein 84 C5H8O 000922-63-4 45 4 2-Butenal, 3-methyl- 84 C5H8O 000107-86-8 42 Abundance

69 (s) Scan 207 (6.940 min): 1040.D (-) m/z 83.95 100.00%

5000

12 69 6.60 6.80 7.00 7.20 ■ ’ । ’ •' ■ ।1 ■' ■ । '11 ■ .4+474 -+ । ■1 j ■ • ■ 11 > ■ ■ ■ i ■ • • ■ i ■ ■ - m/z 55.00 ‘ 82.03% m/z- 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 1 Abundance #574: 2-Butenal, 2-methyi - 55 84 27

5000- 39 PB—nn—CTurut— i 6.60 6.80 7.00 7.20 i m/z 39.05 74.92% 51 ■ i1 1 ■ i11' ■ i1'111 rtsssvivtttgtss"sdtsdso"sspow**"*‘II/‘I‘ mz-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 Aba . c) 39 55

83 ' A, । w ! 6.60 ' m/z 6.80 41.05 ' A7.00 7.20 _ 67.97% 5000 27 51 65 69 TIPnmuBPuTIT mi. - Abundance 20 25 30 35 40 45 50 55 60 65 #551: 2-Ethylacrolein 70 75 80 85 90 ' vwwWW A ’ ' I ' 1 1 ' I 1 1 ' ' I 55—---- 6.60 6.80 7.00 7.20 _ 84 m/ z 83 .05 " 53.12% 5000- 39 27

- r I I—n‘‘m66—nIInTDTTTTT 44 51 TI‘ ' i' ■ ' i1'' ' i' 11417" 1' r M/2.. > 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 6.60 6.80 7.00 7.20

1040.D GCMS0208.M Tue Feb 19 10:33:53 2002 Page 2

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