GCMS analysis results for sample AE11602, June 2002

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\MAY2102\11602.D Vial: 31 Acq On : 22 May 2002 8:06 pm Operator: Sample : EXTRACTS/20 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0520 .M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 6 1-Octene, 3-ethyl- Concentration Rank 13 R.T. EstConc Area Relative to ISTD R.T. 10.35 0.88 ug/1 56412 1,4-Dichlorobenzene-d4 12.15 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 1-Octene, 3-ethyl- 140 C10H20 074630-08-3 38 2 1-Hexanol, 3-methyl- 116 C7H160 013231-81-7 36 3 Hexan 2,3-dimethyl- 114 C8H18 000584-94-1 9 4 Butan 2-cyclopropyl- 98 C7H14 005750-02-7 9 Abundance * Scan 579 (10.350 min): 11602.D (-) m/z 43.05 100.00% 43 70

55 5000

10.00 10.20 10.40 10.60 111 — J k... 3001 m/z 70.05 84.42%

Mu miz-> 20 40 50 60 70 80 90 100 110 120 130 140 Abundance #7585: 1-Octene, 3-ethyl- 43 70

55 5000 10.00 10.20 10.40 10.60 1 ‘1 ‘ 27 m/z 69.10 60.72% - 84 111 140 ’’11//11/11/1//1///7111/1/—/rd/1/“/-/-1///t/r/rI/E37 niz-> 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #3374:1-Hexanol, 3-methyl- 43 55 70 10.00 10.20 10.40 10.60

A 5000 m/ Z 55.10 52.87% 31 83 T-r-p-r ' i 1 ■ ‘ I' ‘ ‘ ' I ' ' ‘ 1 I ‘ ‘ ' I ‘ ' ‘ I ' ' ‘ ‘ 1 1 ' ''I‘' miz-> 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #3097: Hexane, 2,3-dimethyl- ■ ■ i • ■ ‘ I ' ■ ‘ ' I ' ‘ ' I ‘ ‘ ‘ I ' 43 10.00 10.20 10,40 10.60 m/z 41.15 37.29% 70 5000

miz—> 27

' i ■ ■ ■ ■ i ■1 ■ ■ I' 20 30 40 1 ‘ 55

। ■ ■ ■•।■I1 50 60 70 85 80’ 9o 100/110 120 130 140 114 M 10.00 10.20 10.40 10.60

11602.D GCMS0520.M Fri May 24 08:33:10 2002 Page 6

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